(S)-methyl 2-(N-((S)-2-(4-methylphenylsulfonamido)propyl)methylsulfonamido)propanoate

Base Information

Chemical Name:(S)-methyl 2-(N-((S)-2-(4-methylphenylsulfonamido)propyl)methylsulfonamido)propanoate
CAS No.:1264148-78-8
Molecular Formula:C₁₅H₂₄N₂O₆S₂
Molecular Weight:392.497
Hs Code.:

Synonyms:(S)-methyl 2-(N-((S)-2-(4-methylphenylsulfonamido)propyl)methylsulfonamido)propanoate

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Chemical Property of (S)-methyl 2-(N-((S)-2-(4-methylphenylsulfonamido)propyl)methylsulfonamido)propanoate

Chemical Property:

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Technology Process of (S)-methyl 2-(N-((S)-2-(4-methylphenylsulfonamido)propyl)methylsulfonamido)propanoate

There total 4 articles about (S)-methyl 2-(N-((S)-2-(4-methylphenylsulfonamido)propyl)methylsulfonamido)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1264148-57-3
(S)-methyl 2((S)-2-(4-methylphenylsulfonamido)propylamino)propanoate

: 124-63-0
methanesulfonyl chloride

: 1264148-78-8
(S)-methyl 2-(N-((S)-2-(4-methylphenylsulfonamido)propyl)methylsulfonamido)propanoate

Guidance literature:: With pyridine; at 0 - 20 ℃;
DOI:10.1002/asia.201000554

Reference yield:

: 119461-40-4
S-(+)-2-methyl-N-p-tosylaziridine

: 1264148-78-8
(S)-methyl 2-(N-((S)-2-(4-methylphenylsulfonamido)propyl)methylsulfonamido)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / tetrahydrofuran / 0.08 h / 0 °C

1.2: 0 - 60 °C

2.1: pyridine / 0 - 20 °C

With pyridine; triethylamine; In tetrahydrofuran;
DOI:10.1002/asia.201000554

Reference yield:

: 59724-69-5
(S)-N-tosylalanine methyl ester

: 1264148-78-8
(S)-methyl 2-(N-((S)-2-(4-methylphenylsulfonamido)propyl)methylsulfonamido)propanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium borohydride / tetrahydrofuran / 0 - 20 °C

2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

3.1: triethylamine / tetrahydrofuran / 0.08 h / 0 °C

3.2: 0 - 60 °C

4.1: pyridine / 0 - 20 °C

With pyridine; lithium borohydride; triethylamine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 2.1: Mitsunobu cyclization;
DOI:10.1002/asia.201000554