2,2'-diamino-3,3',4,4',6,6'-hexafluorodiphenyl diselenide

Base Information

Chemical Name:2,2'-diamino-3,3',4,4',6,6'-hexafluorodiphenyl diselenide
CAS No.:1274916-51-6
Molecular Formula:C₁₂H₆F₆N₂Se₂
Molecular Weight:450.103
Hs Code.:

Synonyms:2,2'-diamino-3,3',4,4',6,6'-hexafluorodiphenyl diselenide

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Chemical Property of 2,2'-diamino-3,3',4,4',6,6'-hexafluorodiphenyl diselenide

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Technology Process of 2,2'-diamino-3,3',4,4',6,6'-hexafluorodiphenyl diselenide

There total 4 articles about 2,2'-diamino-3,3',4,4',6,6'-hexafluorodiphenyl diselenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1274916-32-3
5,6,8-trifluoro-3,1,2,4-benzothiaselenadiazine

: 1274916-51-6
2,2'-diamino-3,3',4,4',6,6'-hexafluorodiphenyl diselenide

Guidance literature:: With hydrogenchloride; In diethyl ether; water; for 24h;
DOI:10.1021/ic102565x

Reference yield:

: 1274916-46-9
2,3,4,6-tetrafluorophenylselenenyl chloride

: 1274916-51-6
2,2'-diamino-3,3',4,4',6,6'-hexafluorodiphenyl diselenide

Guidance literature:: Multi-step reaction with 3 steps

1: hexane / 2 h / -30 - 20 °C / Inert atmosphere

2: cesium fluoride / acetonitrile / 2 h / Inert atmosphere; Reflux

3: hydrogenchloride / diethyl ether; water / 24 h

With hydrogenchloride; cesium fluoride; In diethyl ether; hexane; water; acetonitrile;
DOI:10.1021/ic102565x

Reference yield:

: 1274916-44-7
1-(2,3,4,6-tetrafluorophenyl)-4-trimethylsilyl-2,4-diaza-1-selena-3-thia-2,3-butadiene

: 1274916-51-6
2,2'-diamino-3,3',4,4',6,6'-hexafluorodiphenyl diselenide

Guidance literature:: Multi-step reaction with 2 steps

1: cesium fluoride / acetonitrile / 2 h / Inert atmosphere; Reflux

2: hydrogenchloride / diethyl ether; water / 24 h

With hydrogenchloride; cesium fluoride; In diethyl ether; water; acetonitrile;
DOI:10.1021/ic102565x