1-(2,3,4,6-tetrafluorophenyl)-4-trimethylsilyl-2,4-diaza-1-selena-3-thia-2,3-butadiene

Base Information

Chemical Name:1-(2,3,4,6-tetrafluorophenyl)-4-trimethylsilyl-2,4-diaza-1-selena-3-thia-2,3-butadiene
CAS No.:1274916-44-7
Molecular Formula:C₉H₁₀F₄N₂SSeSi
Molecular Weight:361.297
Hs Code.:

Synonyms:1-(2,3,4,6-tetrafluorophenyl)-4-trimethylsilyl-2,4-diaza-1-selena-3-thia-2,3-butadiene

Suppliers and Price of 1-(2,3,4,6-tetrafluorophenyl)-4-trimethylsilyl-2,4-diaza-1-selena-3-thia-2,3-butadiene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-(2,3,4,6-tetrafluorophenyl)-4-trimethylsilyl-2,4-diaza-1-selena-3-thia-2,3-butadiene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(2,3,4,6-tetrafluorophenyl)-4-trimethylsilyl-2,4-diaza-1-selena-3-thia-2,3-butadiene

There total 2 articles about 1-(2,3,4,6-tetrafluorophenyl)-4-trimethylsilyl-2,4-diaza-1-selena-3-thia-2,3-butadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 503027-47-2,503027-48-3,155139-78-9,18156-25-7
N,N'-bis(trimethylsilyl)sulfurdiimide

: 1274916-46-9
2,3,4,6-tetrafluorophenylselenenyl chloride

: 1274916-44-7
1-(2,3,4,6-tetrafluorophenyl)-4-trimethylsilyl-2,4-diaza-1-selena-3-thia-2,3-butadiene

Guidance literature:: In hexane; at -30 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ic102565x

Reference yield:

: 2367-82-0
1,2,3,5-tetrafluorobenzene

: 1274916-44-7
1-(2,3,4,6-tetrafluorophenyl)-4-trimethylsilyl-2,4-diaza-1-selena-3-thia-2,3-butadiene

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / diethyl ether; hexane / 1 h / -60 °C / Inert atmosphere

1.2: -60 - 20 °C / Inert atmosphere

2.1: sulfuryl dichloride / 1 h / Reflux

3.1: hexane / 2 h / -30 - 20 °C / Inert atmosphere

With n-butyllithium; sulfuryl dichloride; In diethyl ether; hexane;
DOI:10.1021/ic102565x

Reference yield:

: 1274916-44-7
1-(2,3,4,6-tetrafluorophenyl)-4-trimethylsilyl-2,4-diaza-1-selena-3-thia-2,3-butadiene

: 1274916-66-3
C₂₄H₁₆F₃N₂PSSe

Guidance literature:: Multi-step reaction with 2 steps

1: cesium fluoride / acetonitrile / 2 h / Inert atmosphere; Reflux

2: toluene / 1.5 h / -70 °C / Inert atmosphere

With cesium fluoride; In toluene; acetonitrile;
DOI:10.1021/ic102565x