(1S,2S,6R)-3-methyl-6-(prop-1-en-2-yl)cyclohex-3-ene-1,2-diyl dinicotinate

Base Information

Chemical Name:(1S,2S,6R)-3-methyl-6-(prop-1-en-2-yl)cyclohex-3-ene-1,2-diyl dinicotinate
CAS No.:1361947-97-8
Molecular Formula:C₂₂H₂₂N₂O₄
Molecular Weight:378.428
Hs Code.:

Synonyms:(1S,2S,6R)-3-methyl-6-(prop-1-en-2-yl)cyclohex-3-ene-1,2-diyl dinicotinate

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Chemical Property of (1S,2S,6R)-3-methyl-6-(prop-1-en-2-yl)cyclohex-3-ene-1,2-diyl dinicotinate

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Technology Process of (1S,2S,6R)-3-methyl-6-(prop-1-en-2-yl)cyclohex-3-ene-1,2-diyl dinicotinate

There total 6 articles about (1S,2S,6R)-3-methyl-6-(prop-1-en-2-yl)cyclohex-3-ene-1,2-diyl dinicotinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 1307886-98-1
(1S,2S,6R)-3-methyl-6-(1-methylethenyl)cyclohex-3-ene-1,2-diol

: 20260-53-1
pyridine-3-carbonyl chloride hydrochloride

: 1361947-93-4
(1S,5R,6S)-6-hydroxy-2-methyl-5-(prop-1-en-2-yl)cyclohex-2-enyl nicotinate

: 1361947-97-8
(1S,2S,6R)-3-methyl-6-(prop-1-en-2-yl)cyclohex-3-ene-1,2-diyl dinicotinate

Guidance literature:: With dmap; triethylamine; In diethyl ether; for 24h;
DOI:10.2174/157018011794839411

Reference yield:

: 473-67-6,1820-09-3,1845-30-3,5416-53-5,13040-03-4,18881-04-4,19890-02-9,22339-08-8,80795-83-1
(1R,5R)-4,6,6-trimethylbicyclo[3.1.1]hept-3-en-2-ol

: 1361947-93-4
(1S,5R,6S)-6-hydroxy-2-methyl-5-(prop-1-en-2-yl)cyclohex-2-enyl nicotinate

: 1361947-97-8
(1S,2S,6R)-3-methyl-6-(prop-1-en-2-yl)cyclohex-3-ene-1,2-diyl dinicotinate

Guidance literature:: Multi-step reaction with 5 steps

1: Cr₂HO₇^(2-)*Na⁽³⁺⁾; sulfuric acid

2: dihydrogen peroxide; sodium hydroxide / methanol / 2 h / 10 - 13 °C

3: lithium aluminium tetrahydride / diethyl ether / 2.75 h / 0 °C

4: clay K₁₀ / dichloromethane / 1 h / 20 °C

5: dmap; triethylamine / diethyl ether / 24 h

With dmap; lithium aluminium tetrahydride; sulfuric acid; Cr₂HO₇^(2-)*Na⁽³⁺⁾; dihydrogen peroxide; triethylamine; sodium hydroxide; In methanol; diethyl ether; dichloromethane;
DOI:10.2174/157018011794839411

Reference yield:

: 66885-03-8,90582-89-1
(+)-cis-verbenol epoxide

: 1361947-93-4
(1S,5R,6S)-6-hydroxy-2-methyl-5-(prop-1-en-2-yl)cyclohex-2-enyl nicotinate

: 1361947-97-8
(1S,2S,6R)-3-methyl-6-(prop-1-en-2-yl)cyclohex-3-ene-1,2-diyl dinicotinate

Guidance literature:: Multi-step reaction with 2 steps

1: clay K₁₀ / dichloromethane / 1 h / 20 °C

2: dmap; triethylamine / diethyl ether / 24 h

With dmap; triethylamine; In diethyl ether; dichloromethane;
DOI:10.2174/157018011794839411