3-(tert-butyldimethylsiloxy)-2-methylcyclohex-1-enyl trifluoromethanesulfonate

Base Information

Chemical Name:3-(tert-butyldimethylsiloxy)-2-methylcyclohex-1-enyl trifluoromethanesulfonate
CAS No.:197292-38-9
Molecular Formula:C₁₄H₂₅F₃O₄SSi
Molecular Weight:374.497
Hs Code.:

Synonyms:3-(tert-butyldimethylsiloxy)-2-methylcyclohex-1-enyl trifluoromethanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(tert-butyldimethylsiloxy)-2-methylcyclohex-1-enyl trifluoromethanesulfonate

Chemical Property:

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Technology Process of 3-(tert-butyldimethylsiloxy)-2-methylcyclohex-1-enyl trifluoromethanesulfonate

There total 3 articles about 3-(tert-butyldimethylsiloxy)-2-methylcyclohex-1-enyl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1193-55-1
2-methylcyclohexane-1,3-dione

: 197292-38-9
3-(tert-butyldimethylsiloxy)-2-methylcyclohex-1-enyl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / NaH / tetrahydrofuran; dimethylformamide / 1.) 0 deg C, 30 min, 2.) r.t., 30 min

2: NaBH₄ / methanol / 0.25 h / 0 °C

3: Et₃N, DMAP / CH₂Cl₂ / 5 h / Ambient temperature

With dmap; sodium tetrahydroborate; sodium hydride; triethylamine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/a702815f

Reference yield:

: 150765-78-9
2-methyl-3-oxocyclohex-1-en-1-yl trifluoromethanesulfonate

: 197292-38-9
3-(tert-butyldimethylsiloxy)-2-methylcyclohex-1-enyl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / methanol / 0.25 h / 0 °C

2: Et₃N, DMAP / CH₂Cl₂ / 5 h / Ambient temperature

With dmap; sodium tetrahydroborate; triethylamine; In methanol; dichloromethane;
DOI:10.1039/a702815f