C₃₂H₄₂ClNO₄Sn

Base Information

• Chemical Name: C₃₂H₄₂ClNO₄Sn
• CAS No.: 1017280-65-7
• Molecular Formula: C₃₂H₄₂ClNO₄Sn
• Molecular Weight: 658.853
• Mol file: 1017280-65-7.mol

Synonyms:C₃₂H₄₂ClNO₄Sn

Chemical Property of C₃₂H₄₂ClNO₄Sn

Chemical Property:

Purity/Quality:

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Technology Process of C₃₂H₄₂ClNO₄Sn

There total 1 articles about C₃₂H₄₂ClNO₄Sn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

O2N(Cl)C6H3C6H2(OBn)(OH)SnBu3 (1017280-59-9) + methyl iodide (74-88-4) → C32H42ClNO4Sn (1017280-65-7)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide;

Reference yield: 95.0%

C32H42ClNO4Sn (1017280-65-7) → C20H15ClINO4 (1017280-66-8)

Guidance literature:

With iodine; In toluene; at 20 ℃; for 2h;

DOI:10.1021/ja7113486

Reference yield:

C32H42ClNO4Sn (1017280-65-7) → C26H20ClNO4 (1017280-68-0)

Guidance literature:

Multi-step reaction with 2 steps

1: iodine / toluene

2: caesium carbonate / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tricyclohexylphosphine / 1,4-dioxane / 80 °C

With iodine; caesium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tricyclohexylphosphine; In 1,4-dioxane; toluene;

upstream raw materials:

O₂N(Cl)C₆H₃C₆H₂(OBn)(OH)SnBu₃

methyl iodide

Downstream raw materials:

C₂₀H₁₅ClINO₄

C₂₁H₁₈ClNO₄

C₂₂H₂₁NO₄

C₂₆H₂₀ClNO₄