N-(6-(4-(methylsulfonyl)phenoxy)-5-((tetrahydrofuran-3-yl)methyl)pyridin-3-yl)pyridin-2-amine

Base Information

Chemical Name:N-(6-(4-(methylsulfonyl)phenoxy)-5-((tetrahydrofuran-3-yl)methyl)pyridin-3-yl)pyridin-2-amine
CAS No.:1375458-92-6
Molecular Formula:C₂₂H₂₃N₃O₄S
Molecular Weight:425.508
Hs Code.:

Synonyms:N-(6-(4-(methylsulfonyl)phenoxy)-5-((tetrahydrofuran-3-yl)methyl)pyridin-3-yl)pyridin-2-amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(6-(4-(methylsulfonyl)phenoxy)-5-((tetrahydrofuran-3-yl)methyl)pyridin-3-yl)pyridin-2-amine

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Technology Process of N-(6-(4-(methylsulfonyl)phenoxy)-5-((tetrahydrofuran-3-yl)methyl)pyridin-3-yl)pyridin-2-amine

There total 5 articles about N-(6-(4-(methylsulfonyl)phenoxy)-5-((tetrahydrofuran-3-yl)methyl)pyridin-3-yl)pyridin-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 109-09-1
2-chloropyridine

: 1375458-98-2
C₁₇H₂₀N₂O₄S

: 1375458-92-6
N-(6-(4-(methylsulfonyl)phenoxy)-5-((tetrahydrofuran-3-yl)methyl)pyridin-3-yl)pyridin-2-amine

Guidance literature:: C₁₇H₂₀N₂O₄S; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 1h;

2-chloropyridine; In N,N-dimethyl-formamide; mineral oil;

With water; In N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1375458-96-0
C₁₀H₁₂N₂O₄

: 1375458-92-6
N-(6-(4-(methylsulfonyl)phenoxy)-5-((tetrahydrofuran-3-yl)methyl)pyridin-3-yl)pyridin-2-amine

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / ethanol / Reflux; Inert atmosphere

2: hydrogen / raney nickel / ethanol / 50 °C / 3040.2 Torr / Inert atmosphere

3: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 20 °C

With hydrogen; sodium hydride; sodium hydrogencarbonate; raney nickel; In ethanol; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1375458-97-1
C₁₇H₁₈N₂O₆S

: 1375458-92-6
N-(6-(4-(methylsulfonyl)phenoxy)-5-((tetrahydrofuran-3-yl)methyl)pyridin-3-yl)pyridin-2-amine

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / raney nickel / ethanol / 50 °C / 3040.2 Torr / Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 20 °C

With hydrogen; sodium hydride; raney nickel; In ethanol; N,N-dimethyl-formamide; mineral oil;