Technology Process of C11H8BrNO3
There total 3 articles about C11H8BrNO3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium hydrogencarbonate; potassium bromide;
In
dichloromethane; water;
at 23 ℃;
for 0.25h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: methanol; sodium tetrahydroborate
2: bromine / tetrahydrofuran / 6 h / 0 °C
3: 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium hydrogencarbonate; potassium bromide / dichloromethane; water / 0.25 h / 23 °C
With
methanol; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium tetrahydroborate; bromine; sodium hydrogencarbonate; potassium bromide;
In
tetrahydrofuran; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: bromine / tetrahydrofuran / 6 h / 0 °C
2: 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium hydrogencarbonate; potassium bromide / dichloromethane; water / 0.25 h / 23 °C
With
2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; bromine; sodium hydrogencarbonate; potassium bromide;
In
tetrahydrofuran; dichloromethane; water;