4,7,7-trimethyl-3-exo-(1-naphthyl)bicyclo<2.2.1>heptan-2-exo-yl 3-cyclohexyl-3-oxopropanoate

Base Information

Chemical Name:4,7,7-trimethyl-3-exo-(1-naphthyl)bicyclo<2.2.1>heptan-2-exo-yl 3-cyclohexyl-3-oxopropanoate
CAS No.:110971-08-9
Molecular Formula:C₂₉H₃₆O₃
Molecular Weight:432.603
Hs Code.:

Synonyms:4,7,7-trimethyl-3-exo-(1-naphthyl)bicyclo<2.2.1>heptan-2-exo-yl 3-cyclohexyl-3-oxopropanoate

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Chemical Property of 4,7,7-trimethyl-3-exo-(1-naphthyl)bicyclo<2.2.1>heptan-2-exo-yl 3-cyclohexyl-3-oxopropanoate

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Technology Process of 4,7,7-trimethyl-3-exo-(1-naphthyl)bicyclo<2.2.1>heptan-2-exo-yl 3-cyclohexyl-3-oxopropanoate

There total 3 articles about 4,7,7-trimethyl-3-exo-(1-naphthyl)bicyclo<2.2.1>heptan-2-exo-yl 3-cyclohexyl-3-oxopropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 64670-15-1
methyl 3-cyclohexyl-3-oxopropionate

: 86835-18-9
(4S)-3-exo-(1-naphthyl)-4,7,7-trimethylbicyclo[2.2.1]heptan-2-exo-ol

: 110971-08-9
4,7,7-trimethyl-3-exo-(1-naphthyl)bicyclo<2.2.1>heptan-2-exo-yl 3-cyclohexyl-3-oxopropanoate

Guidance literature:: With dmap; In toluene; for 40h; Heating;
DOI:10.1021/ja00258a039

Reference yield:

: 2719-27-9
cyclohexanylcarbonyl chloride

: 110971-08-9
4,7,7-trimethyl-3-exo-(1-naphthyl)bicyclo<2.2.1>heptan-2-exo-yl 3-cyclohexyl-3-oxopropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / LDA / tetrahydrofuran / -78 °C

2: 99 percent / 4-DMAP / toluene / 40 h / Heating

With dmap; lithium diisopropyl amide; In tetrahydrofuran; toluene;
DOI:10.1021/ja00258a039

Reference yield:

: 98-89-5
Cyclohexanecarboxylic acid

: 110971-08-9
4,7,7-trimethyl-3-exo-(1-naphthyl)bicyclo<2.2.1>heptan-2-exo-yl 3-cyclohexyl-3-oxopropanoate

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride / dimethylformamide; CH₂Cl₂ / 1.) 0 deg C, 2.) RT, 3 h

2: 87 percent / LDA / tetrahydrofuran / -78 °C

3: 99 percent / 4-DMAP / toluene / 40 h / Heating

With dmap; oxalyl dichloride; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja00258a039