O₂-(2,4-dinitrophenyl) 1-[4-homopiperazin-1-yl]diazen-1-ium-1,2-diolate hydrochloride

Base Information

• Chemical Name: O₂-(2,4-dinitrophenyl) 1-[4-homopiperazin-1-yl]diazen-1-ium-1,2-diolate hydrochloride
• CAS No.: 1163704-89-9
• Molecular Formula: C₁₁H₁₄N₆O₆*ClH
• Molecular Weight: 362.73

Synonyms:O₂-(2,4-dinitrophenyl) 1-[4-homopiperazin-1-yl]diazen-1-ium-1,2-diolate hydrochloride

Chemical Property of O₂-(2,4-dinitrophenyl) 1-[4-homopiperazin-1-yl]diazen-1-ium-1,2-diolate hydrochloride

Chemical Property:

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Technology Process of O₂-(2,4-dinitrophenyl) 1-[4-homopiperazin-1-yl]diazen-1-ium-1,2-diolate hydrochloride

There total 1 articles about O₂-(2,4-dinitrophenyl) 1-[4-homopiperazin-1-yl]diazen-1-ium-1,2-diolate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

O2-(2,4-dinitrophenyl) 1-[(4-t-butoxycarbonyl)homopiperazin-1-yl]diazen-1-ium-1,2-diolate (1163704-88-8) → O2-(2,4-dinitrophenyl) 1-[4-homopiperazin-1-yl]diazen-1-ium-1,2-diolate hydrochloride (1163704-89-9)

Guidance literature:

With hydrogenchloride; In water; ethyl acetate; at 20 ℃; Ice cooling;

DOI:10.1016/j.bmcl.2009.03.115

Reference yield: 89.0%

propargyl chloroformate (35718-08-2) + O2-(2,4-dinitrophenyl) 1-[4-homopiperazin-1-yl]diazen-1-ium-1,2-diolate hydrochloride (1163704-89-9) → O2-(2,4-dinitrophenyl) 1-[4-(allyloxycarbonyl)homopiperazin-1-yl]diazen-1-ium-1,2-diolate (1163704-83-3)

Guidance literature:

With triethylamine; In dichloromethane;

DOI:10.1016/j.bmcl.2009.03.115

Reference yield: 89.0%

2-fluoroethyl chloroformate (462-27-1) + O2-(2,4-dinitrophenyl) 1-[4-homopiperazin-1-yl]diazen-1-ium-1,2-diolate hydrochloride (1163704-89-9) → O2-(2,4-dinitrophenyl) 1-[4-(2-fluoroethoxycarbonyl)homopiperazin-1-yl]diazen-1-ium-1,2-diolate (1163704-79-7)

Guidance literature:

With triethylamine; In dichloromethane;

DOI:10.1016/j.bmcl.2009.03.115

upstream raw materials:

O₂-(2,4-dinitrophenyl) 1-[(4-t-butoxycarbonyl)homopiperazin-1-yl]diazen-1-ium-1,2-diolate

Downstream raw materials:

O₂-(2,4-dinitrophenyl) 1-[4-(vinyloxycarbonyl)homopiperazin-1-yl]diazen-1-ium-1,2-diolate

O₂-(2,4-dinitrophenyl) 1-[4-(allyloxycarbonyl)homopiperazin-1-yl]diazen-1-ium-1,2-diolate

O₂-(2,4-dinitrophenyl) 1-[4-(2-fluoroethoxycarbonyl)homopiperazin-1-yl]diazen-1-ium-1,2-diolate

O₂-(2,4-dinitrophenyl) 1-[4-(ethylmercaptocarbonyl)homopiperazin-1-yl]diazen-1-ium-1,2-diolate

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