TETRAKIS(SPIROCYCLOHEXANE)CALIX(4)PYRROLE

Base Information

• Chemical Name: TETRAKIS(SPIROCYCLOHEXANE)CALIX(4)PYRROLE
• CAS No.: 35320-70-8
• Molecular Formula: C₄₀H₅₂N₄
• Molecular Weight: 588.88
• Mol file: 35320-70-8.mol

Synonyms:Tetraspiro[21,22,23,24-tetraazapentacyclo[16.2.1.13,6.18,11.113,16]tetracosa-3,5,8,10,13,15,18,20-octaene-2,1':7,1'':12,1''':17,1''''-tetrakiscyclohexane];meso-Tetracyclohexylcalix[4]pyrrole

Chemical Property of TETRAKIS(SPIROCYCLOHEXANE)CALIX(4)PYRROLE

Chemical Property:

• PSA: 63.16000
• LogP: 10.31320

Purity/Quality:

99% ^*data from raw suppliers

TETRAKIS(SPIROCYCLOHEXANE)CALIX(4)PYRROLE 95.00% ^*data from reagent suppliers

Safty Information:

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Technology Process of TETRAKIS(SPIROCYCLOHEXANE)CALIX(4)PYRROLE

There total 3 articles about TETRAKIS(SPIROCYCLOHEXANE)CALIX(4)PYRROLE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.3%

pyrrole (109-97-7,30604-81-0) + cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → tetraspirocyclohexyl calix(4)pyrrole (35320-70-8) + 2,2'-(cyclohexane-1,1-diyl)bis(1H-pyrrole) (35303-46-9) + 2,5-Bis-[1-(1H-pyrrol-2-yl)-cyclohexyl]-1H-pyrrole + C34H44N4

Guidance literature:

With molecular sieve; In dichloromethane; for 10h; Further Variations:; Reagents; Product distribution; Heating;

DOI:10.1039/b105690p

Reference yield: 21.9%

pyrrole (109-97-7,30604-81-0) + cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + acetone (67-64-1) → tetraspirocyclohexyl calix(4)pyrrole (35320-70-8) + 5,5'-dimethyldipyrromethane (99840-54-7) + 5,10,15,20,22,24-hexahydro-5,5,10,10,15,15,20,20-octamethyl-21H,23H-porphine (4475-42-7) + C34H44N4

Guidance literature:

With molecular sieve; In dichloromethane; for 10h; Further byproducts.; Heating;

DOI:10.1039/b105690p

Reference yield:

pyrrole (109-97-7,30604-81-0) + cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → tetraspirocyclohexyl calix(4)pyrrole (35320-70-8) + 2,2'-(cyclohexane-1,1-diyl)bis(1H-pyrrole) (35303-46-9)

Guidance literature:

With HZSM-5⁽³⁰⁾; In dichloromethane; at 20 ℃; for 10h;

DOI:10.3390/molecules16097256

upstream raw materials:

pyrrole

cyclohexanone

acetone

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