1,3-di-(2-anisidyl)-4,5,6,7-tetrahydro-3H-[1,3]diazepinium tetrafluoroborate

Base Information

Chemical Name:1,3-di-(2-anisidyl)-4,5,6,7-tetrahydro-3H-[1,3]diazepinium tetrafluoroborate
CAS No.:1192371-06-4
Molecular Formula:BF₄*C₁₉H₂₃N₂O₂
Molecular Weight:398.208
Hs Code.:

Synonyms:1,3-di-(2-anisidyl)-4,5,6,7-tetrahydro-3H-[1,3]diazepinium tetrafluoroborate

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Chemical Property of 1,3-di-(2-anisidyl)-4,5,6,7-tetrahydro-3H-[1,3]diazepinium tetrafluoroborate

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Technology Process of 1,3-di-(2-anisidyl)-4,5,6,7-tetrahydro-3H-[1,3]diazepinium tetrafluoroborate

There total 1 articles about 1,3-di-(2-anisidyl)-4,5,6,7-tetrahydro-3H-[1,3]diazepinium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1192371-32-6
1,3-di(2-anisidyl)-4,5,6,7-tetrahydro-3H-[1,3]diazepinium iodide

: 1192371-06-4
1,3-di-(2-anisidyl)-4,5,6,7-tetrahydro-3H-[1,3]diazepinium tetrafluoroborate

Guidance literature:: With sodium tetrafluoroborate; In water; acetonitrile; Inert atmosphere;
DOI:10.1039/b909834h

Reference yield: 50.0%

: chloro(1,5-cyclooctadiene)rhodium(I) dimer

: 1192371-06-4
1,3-di-(2-anisidyl)-4,5,6,7-tetrahydro-3H-[1,3]diazepinium tetrafluoroborate

: Rh(C₅H₈N₂(C₆H₄OCH₃)2)(C₈H₁₂)Cl

Guidance literature:: With KN(Si(CH₃)3)2; In tetrahydrofuran; under Ar; THF added to mixt. of KN(SiMe3)2 and BF4 salt of ligand; stirred for 30 min; filtered to THF soln. of Rh complex; stirred at room temp. for 2 h; volatiles removed in vac.; solid washed with hexane; dried; elem. anal.;
DOI:10.1039/b909834h