spiro-3-carboxylic acid, methyl ester

Base Information

Chemical Name:spiro-3-carboxylic acid, methyl ester
CAS No.:89908-85-0
Molecular Formula:C₁₇H₂₂O₃Se
Molecular Weight:353.32
Hs Code.:

spiro<tetrahydrofuran-2(3H),1',2'-(phenylseleno)cyclohexane>-3-carboxylic acid, methyl ester

Synonyms:spiro-3-carboxylic acid, methyl ester

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Chemical Property of spiro-3-carboxylic acid, methyl ester

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Technology Process of spiro-3-carboxylic acid, methyl ester

There total 5 articles about spiro-3-carboxylic acid, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 5707-04-0
Phenylselenyl chloride

: 89908-81-6
2-(cyclohex-1-enyl)-4-hydroxybutanoic acid, methyl ester

: 89908-85-0
spiro-3-carboxylic acid, methyl ester

Guidance literature:: In dichloromethane; at -78 ℃; for 1h;
DOI:10.1021/jo00187a031

Reference yield:

: 32591-07-4
α-(cyclohex-1-enyl)-γ-butyrolactone

: 89908-85-0
spiro-3-carboxylic acid, methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / 2 N NaOH / 0.75 h / Heating

2: 82.9 percent / diethyl ether

3: 99 percent / CH₂Cl₂ / 1 h / -78 °C

With sodium hydroxide; In diethyl ether; dichloromethane;
DOI:10.1021/jo00187a031

Reference yield:

: 61097-33-4
α-(1-hydroxycyclohexyl)-γ-butyrolactone

: 89908-85-0
spiro-3-carboxylic acid, methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 97.4 percent / P₂O₅, Celite / benzene / 12 h

2: 100 percent / 2 N NaOH / 0.75 h / Heating

3: 82.9 percent / diethyl ether

4: 99 percent / CH₂Cl₂ / 1 h / -78 °C

With sodium hydroxide; Celite; phosphorus pentoxide; In diethyl ether; dichloromethane; benzene;
DOI:10.1021/jo00187a031