3-N-(ethylamino)-N’-[2-bromo-6-chloro-4-(1,1,1,2,3,3,3-(heptafluoro)propyl)phenyl]-2-methoxybenzamide

Base Information

Chemical Name:3-N-(ethylamino)-N’-[2-bromo-6-chloro-4-(1,1,1,2,3,3,3-(heptafluoro)propyl)phenyl]-2-methoxybenzamide
CAS No.:1429514-53-3
Molecular Formula:C₁₉H₁₅BrClF₇N₂O₂
Molecular Weight:551.686
Hs Code.:

Synonyms:3-N-(ethylamino)-N’-[2-bromo-6-chloro-4-(1,1,1,2,3,3,3-(heptafluoro)propyl)phenyl]-2-methoxybenzamide

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Chemical Property of 3-N-(ethylamino)-N’-[2-bromo-6-chloro-4-(1,1,1,2,3,3,3-(heptafluoro)propyl)phenyl]-2-methoxybenzamide

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Technology Process of 3-N-(ethylamino)-N’-[2-bromo-6-chloro-4-(1,1,1,2,3,3,3-(heptafluoro)propyl)phenyl]-2-methoxybenzamide

There total 5 articles about 3-N-(ethylamino)-N’-[2-bromo-6-chloro-4-(1,1,1,2,3,3,3-(heptafluoro)propyl)phenyl]-2-methoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1429514-50-0
3-amino-N-[2-bromo-6-chloro-4-(1,1,1,2,3,3,3-heptafluoroprop-2-yl)phenyl]-2-methoxybenzamide

: 75-07-0,9002-91-9
acetaldehyde

: 1429514-53-3
3-N-(ethylamino)-N’-[2-bromo-6-chloro-4-(1,1,1,2,3,3,3-(heptafluoro)propyl)phenyl]-2-methoxybenzamide

Guidance literature:: With sodium cyanoborohydride; acetic acid; In methanol; at 20 ℃; for 1h;

Reference yield:

: 1429514-43-1
N-[2-bromo-6-chloro-4-(1,1,1,2,3,3,3-(heptafluoro)propyl)phenyl]-2-methoxy-3-nitro-benzamide

: 1429514-53-3
3-N-(ethylamino)-N’-[2-bromo-6-chloro-4-(1,1,1,2,3,3,3-(heptafluoro)propyl)phenyl]-2-methoxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutylammomium bromide; sodium dithionite; sodium hydroxide / tetrahydrofuran / 4 h / Reflux

2: acetic acid; sodium cyanoborohydride / methanol / 1 h / 20 °C

With sodium dithionite; tetrabutylammomium bromide; sodium cyanoborohydride; acetic acid; sodium hydroxide; In tetrahydrofuran; methanol;

Reference yield:

: 317-46-4
2-fluoro-3-nitro-benzoic acid

: 1429514-53-3
3-N-(ethylamino)-N’-[2-bromo-6-chloro-4-(1,1,1,2,3,3,3-(heptafluoro)propyl)phenyl]-2-methoxybenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: N,N-dimethyl-formamide; oxalyl dichloride / 1,2-dichloro-ethane / 20 - 50 °C

2: triethylamine / 1,2-dichloro-ethane / 4 h / Reflux

3: sodium hydroxide; tetrabutylammomium bromide; sodium dithionite / tetrahydrofuran / 4 h / Reflux

4: methanol; acetic acid; sodium cyanoborohydride / 1 h / 20 °C

With methanol; sodium dithionite; oxalyl dichloride; tetrabutylammomium bromide; sodium cyanoborohydride; acetic acid; triethylamine; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran; 1,2-dichloro-ethane;