N-({3-(methyloxy)-5-[3-(methyloxy)propyl]phenyl}methyl)cyclopropanamine

Base Information

Chemical Name:N-({3-(methyloxy)-5-[3-(methyloxy)propyl]phenyl}methyl)cyclopropanamine
CAS No.:1194486-83-3
Molecular Formula:C₁₅H₂₃NO₂
Molecular Weight:249.353
Hs Code.:

Synonyms:N-({3-(methyloxy)-5-[3-(methyloxy)propyl]phenyl}methyl)cyclopropanamine

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Chemical Property of N-({3-(methyloxy)-5-[3-(methyloxy)propyl]phenyl}methyl)cyclopropanamine

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Technology Process of N-({3-(methyloxy)-5-[3-(methyloxy)propyl]phenyl}methyl)cyclopropanamine

There total 7 articles about N-({3-(methyloxy)-5-[3-(methyloxy)propyl]phenyl}methyl)cyclopropanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1229246-24-5
N-({3-(methyloxy)-5-[(1E)-3-(methyloxy)-1-propen-1-yl]phenyl}methyl)-cyclopropanamine

: 1194486-83-3
N-({3-(methyloxy)-5-[3-(methyloxy)propyl]phenyl}methyl)cyclopropanamine

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In ethyl acetate; for 1.5h;

Reference yield:

: 1026786-84-4
3-hydroxy-5-[(1E)-3-(methyloxy)-1-propen-1-yl]benzaldehyde

: 1194486-83-3
N-({3-(methyloxy)-5-[3-(methyloxy)propyl]phenyl}methyl)cyclopropanamine

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / acetone / 16 h / Heating; Reflux

2: magnesium sulfate / dichloromethane / 20 °C

3: magnesium sulfate / dichloromethane / 20 °C

4: sodium tetrahydroborate / methanol / 3.08 h / 0 - 20 °C

5: hydrogen / palladium 10% on activated carbon / ethyl acetate / 1.5 h

With sodium tetrahydroborate; hydrogen; magnesium sulfate; potassium carbonate; palladium 10% on activated carbon; In methanol; dichloromethane; ethyl acetate; acetone;

Reference yield:

: C₁₅H₁₉NO₂

: 1194486-83-3
N-({3-(methyloxy)-5-[3-(methyloxy)propyl]phenyl}methyl)cyclopropanamine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 3.08 h / 0 - 20 °C

2: hydrogen / palladium 10% on activated carbon / ethyl acetate / 1.5 h

With sodium tetrahydroborate; hydrogen; palladium 10% on activated carbon; In methanol; ethyl acetate;