5-(methoxycarbonyl)pentyl 2,4-di-O-benzoyl-3,6-bis-O-(2-deoxy-3,4,6-tri-O-acetyl-2-phthalimido-β-D-glucopyranosyl)-β-D-galactopyranoside

Base Information

Chemical Name:5-(methoxycarbonyl)pentyl 2,4-di-O-benzoyl-3,6-bis-O-(2-deoxy-3,4,6-tri-O-acetyl-2-phthalimido-β-D-glucopyranosyl)-β-D-galactopyranoside
CAS No.:143564-44-7
Molecular Formula:C₆₇H₇₀N₂O₂₈
Molecular Weight:1351.29
Hs Code.:

Synonyms:5-(methoxycarbonyl)pentyl 2,4-di-O-benzoyl-3,6-bis-O-(2-deoxy-3,4,6-tri-O-acetyl-2-phthalimido-β-D-glucopyranosyl)-β-D-galactopyranoside

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Chemical Property of 5-(methoxycarbonyl)pentyl 2,4-di-O-benzoyl-3,6-bis-O-(2-deoxy-3,4,6-tri-O-acetyl-2-phthalimido-β-D-glucopyranosyl)-β-D-galactopyranoside

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Technology Process of 5-(methoxycarbonyl)pentyl 2,4-di-O-benzoyl-3,6-bis-O-(2-deoxy-3,4,6-tri-O-acetyl-2-phthalimido-β-D-glucopyranosyl)-β-D-galactopyranoside

There total 6 articles about 5-(methoxycarbonyl)pentyl 2,4-di-O-benzoyl-3,6-bis-O-(2-deoxy-3,4,6-tri-O-acetyl-2-phthalimido-β-D-glucopyranosyl)-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2233-29-6
2,3,4-lutidine

? molecular sieves: ? molecular sieves

: 70831-94-6
3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-D-glucopyranosyl bromide

: 143564-44-7
5-(methoxycarbonyl)pentyl 2,4-di-O-benzoyl-3,6-bis-O-(2-deoxy-3,4,6-tri-O-acetyl-2-phthalimido-β-D-glucopyranosyl)-β-D-galactopyranoside

Guidance literature:: silver trifluoromethanesulfonate; In 2,3,5-trimethyl-pyridine; nitromethane;

Reference yield:

: 70831-94-6
3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-D-glucopyranosyl bromide

: 134906-99-3
5-(methoxycarbonyl)pentyl 2,4-di-O-benzoyl-β-D-galactopyranoside

: 143564-44-7
5-(methoxycarbonyl)pentyl 2,4-di-O-benzoyl-3,6-bis-O-(2-deoxy-3,4,6-tri-O-acetyl-2-phthalimido-β-D-glucopyranosyl)-β-D-galactopyranoside

Guidance literature:: With 2,3,5-trimethyl-pyridine; silver trifluoromethanesulfonate; In nitromethane;
DOI:10.1021/ja00015a052

Reference yield:

: 98-88-4
benzoyl chloride

: 143564-44-7
5-(methoxycarbonyl)pentyl 2,4-di-O-benzoyl-3,6-bis-O-(2-deoxy-3,4,6-tri-O-acetyl-2-phthalimido-β-D-glucopyranosyl)-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

2: AgOTf, collidine / nitromethane

With 2,3,5-trimethyl-pyridine; silver trifluoromethanesulfonate; In nitromethane;
DOI:10.1021/ja00015a052