tetraethyl 3,9-dibenzyl-6,12-diphenyl-3,9-diazahexacyclo[6.4.0.0(2.7).0(4.11).0(5.10)]dodecane-1,5,7,11-tetracarboxylate

Base Information

• Chemical Name: tetraethyl 3,9-dibenzyl-6,12-diphenyl-3,9-diazahexacyclo[6.4.0.0(2.7).0(4.11).0(5.10)]dodecane-1,5,7,11-tetracarboxylate
• CAS No.: 1053417-68-7
• Molecular Formula: C₄₈H₅₀N₂O₈
• Molecular Weight: 782.934
• Mol file: 1053417-68-7.mol

Synonyms:tetraethyl 3,9-dibenzyl-6,12-diphenyl-3,9-diazahexacyclo[6.4.0.0(2.7).0(4.11).0(5.10)]dodecane-1,5,7,11-tetracarboxylate

Chemical Property of tetraethyl 3,9-dibenzyl-6,12-diphenyl-3,9-diazahexacyclo[6.4.0.0(2.7).0(4.11).0(5.10)]dodecane-1,5,7,11-tetracarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tetraethyl 3,9-dibenzyl-6,12-diphenyl-3,9-diazahexacyclo[6.4.0.0(2.7).0(4.11).0(5.10)]dodecane-1,5,7,11-tetracarboxylate

There total 1 articles about tetraethyl 3,9-dibenzyl-6,12-diphenyl-3,9-diazahexacyclo[6.4.0.0(2.7).0(4.11).0(5.10)]dodecane-1,5,7,11-tetracarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

diethyl 1-benzyl-1,4-dihydro-4-phenylpyridine-3,5-dicarboxylate (120533-76-8) → tetraethyl 3,9-dibenzyl-6,12-diphenyl-3,9-diazahexacyclo[6.4.0.0(2.7).0(4.11).0(5.10)]dodecane-1,5,7,11-tetracarboxylate (1053417-68-7)

Guidance literature:

In tetrahydrofuran; at 20 ℃; Inert atmosphere; UV-irradiation;

DOI:10.1021/jm800480y

Reference yield: 92.0%

tetraethyl 3,9-dibenzyl-6,12-diphenyl-3,9-diazahexacyclo[6.4.0.0(2.7).0(4.11).0(5.10)]dodecane-1,5,7,11-tetracarboxylate (1053417-68-7) → 3,9-dibenzyl-1,5,7,11-tetrakishydroxymethyl-6,12-diphenyl-3,9-diazhexacyclo[6.4.0.02.7.04.11.05.10]dodecane

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 8 ℃; for 3h; Inert atmosphere;

DOI:10.1021/jm800480y

upstream raw materials:

diethyl 1-benzyl-1,4-dihydro-4-phenylpyridine-3,5-dicarboxylate