2-(3,4-dimethoxy-phenyl)-7,8-dimethoxy-2,3,4,5-tetrahydro-1H-benzo[d]azepine

Base Information

Chemical Name:2-(3,4-dimethoxy-phenyl)-7,8-dimethoxy-2,3,4,5-tetrahydro-1H-benzo[d]azepine
CAS No.:792843-84-6
Molecular Formula:C₂₀H₂₅NO₄
Molecular Weight:343.423
Hs Code.:

2-(3,4-dimethoxy-phenyl)-7,8-dimethoxy-2,3,4,5-tetrahydro-1<i>H</i>-benzo[<i>d</i>]azepine

Synonyms:2-(3,4-dimethoxy-phenyl)-7,8-dimethoxy-2,3,4,5-tetrahydro-1H-benzo[d]azepine

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Chemical Property of 2-(3,4-dimethoxy-phenyl)-7,8-dimethoxy-2,3,4,5-tetrahydro-1H-benzo[d]azepine

Chemical Property:

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Technology Process of 2-(3,4-dimethoxy-phenyl)-7,8-dimethoxy-2,3,4,5-tetrahydro-1H-benzo[d]azepine

There total 5 articles about 2-(3,4-dimethoxy-phenyl)-7,8-dimethoxy-2,3,4,5-tetrahydro-1H-benzo[d]azepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 210696-91-6
N-(2-Benzenesulfinyl-ethyl)-N-[1,2-bis-(3,4-dimethoxy-phenyl)-ethyl]-formamide

: 792843-84-6
2-(3,4-dimethoxy-phenyl)-7,8-dimethoxy-2,3,4,5-tetrahydro-1H-benzo[d]azepine

: 13074-31-2
Tetrahydropapaverine

Guidance literature:: Yield given. Multistep reaction. Yields of byproduct given;

Reference yield:

: 4927-55-3
1,2-bis(3,4-dimethoxyphenyl)ethanone

: 792843-84-6
2-(3,4-dimethoxy-phenyl)-7,8-dimethoxy-2,3,4,5-tetrahydro-1H-benzo[d]azepine

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) titanium tetraisopropoxide; 2.) NaBH₄ / 1.) 80 degC, 3 h; 2.) MeOH, rt, 1h

2: 97 percent / acetic anhydride / 1 h / 70 °C

3: 94 percent / sodium metaperiodate / H₂O; methanol / 16 h / Ambient temperature

With titanium(IV) isopropylate; sodium tetrahydroborate; sodium periodate; acetic anhydride; In methanol; water;

Reference yield:

: 148679-64-5
[1,2-Bis-(3,4-dimethoxy-phenyl)-ethyl]-(2-phenylsulfanyl-ethyl)-amine

: 792843-84-6
2-(3,4-dimethoxy-phenyl)-7,8-dimethoxy-2,3,4,5-tetrahydro-1H-benzo[d]azepine

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / acetic anhydride / 1 h / 70 °C

2: 94 percent / sodium metaperiodate / H₂O; methanol / 16 h / Ambient temperature

With sodium periodate; acetic anhydride; In methanol; water;