3-bromo-2,2-bis(4-fluorophenyl)-6-({[(9H-fluoren-9-yl)methoxycarbonyl]amino}methyl)-2H-1-benzopyran

Base Information

Chemical Name:3-bromo-2,2-bis(4-fluorophenyl)-6-({[(9H-fluoren-9-yl)methoxycarbonyl]amino}methyl)-2H-1-benzopyran
CAS No.:1191071-28-9
Molecular Formula:C₃₇H₂₆BrF₂NO₃
Molecular Weight:650.519
Hs Code.:

Synonyms:3-bromo-2,2-bis(4-fluorophenyl)-6-({[(9H-fluoren-9-yl)methoxycarbonyl]amino}methyl)-2H-1-benzopyran

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Chemical Property of 3-bromo-2,2-bis(4-fluorophenyl)-6-({[(9H-fluoren-9-yl)methoxycarbonyl]amino}methyl)-2H-1-benzopyran

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Technology Process of 3-bromo-2,2-bis(4-fluorophenyl)-6-({[(9H-fluoren-9-yl)methoxycarbonyl]amino}methyl)-2H-1-benzopyran

There total 1 articles about 3-bromo-2,2-bis(4-fluorophenyl)-6-({[(9H-fluoren-9-yl)methoxycarbonyl]amino}methyl)-2H-1-benzopyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1191071-25-6
3-bromo-6-({[(9H-fluoren-9-yl)methoxycarbonyl]amino}methyl)-2,2-bis(4-fluorophenyl)-3,4-dihydro-2H-1-benzopyran-4-ol

: 1191071-28-9
3-bromo-2,2-bis(4-fluorophenyl)-6-({[(9H-fluoren-9-yl)methoxycarbonyl]amino}methyl)-2H-1-benzopyran

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 1h; Inert atmosphere; Reflux;
DOI:10.3762/bjoc.5.25

Reference yield: 67.0%

: 557-21-1
zinc(II) cyanide

: 1191071-28-9
3-bromo-2,2-bis(4-fluorophenyl)-6-({[(9H-fluoren-9-yl)methoxycarbonyl]amino}methyl)-2H-1-benzopyran

: 1191071-33-6
3-cyano-2,2-bis(4-fluorophenyl)-6-({[(9H-fluoren-9-yl)methoxycarbonyl]amino}methyl)-2H-1-benzopyran

Guidance literature:: With iodine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; tri tert-butylphosphoniumtetrafluoroborate; zinc; In 1-methyl-pyrrolidin-2-one; at 45 - 65 ℃; Inert atmosphere;
DOI:10.3762/bjoc.5.25

Reference yield: 14.0%

: 201230-82-2
carbon monoxide

: 1191071-28-9
3-bromo-2,2-bis(4-fluorophenyl)-6-({[(9H-fluoren-9-yl)methoxycarbonyl]amino}methyl)-2H-1-benzopyran

: 1191071-34-7
2,2-bis(4-fluorophenyl)-6-({[(9H-fluoren-9-yl)methoxycarbonyl]amino}methyl)-2H-1-benzopyran-3-carboxylic acid

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; water; In tetrahydrofuran; at 100 ℃; under 38002.6 Torr; Molecular sieve; Autoclave;
DOI:10.3762/bjoc.5.25