cyclohexyl 2-acetamido-3-O-benzyl-2-deoxy-(R)-4,6-O-(E-2-methyl-3-phenyl-2-propenylidene)-β-D-glucopyranoside

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Chemical Name:cyclohexyl 2-acetamido-3-O-benzyl-2-deoxy-(R)-4,6-O-(E-2-methyl-3-phenyl-2-propenylidene)-β-D-glucopyranoside
CAS No.:824396-54-5
Molecular Formula:C₃₁H₃₉NO₆
Molecular Weight:521.654
Hs Code.:

Synonyms:cyclohexyl 2-acetamido-3-O-benzyl-2-deoxy-(R)-4,6-O-(E-2-methyl-3-phenyl-2-propenylidene)-β-D-glucopyranoside

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Chemical Property of cyclohexyl 2-acetamido-3-O-benzyl-2-deoxy-(R)-4,6-O-(E-2-methyl-3-phenyl-2-propenylidene)-β-D-glucopyranoside

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Technology Process of cyclohexyl 2-acetamido-3-O-benzyl-2-deoxy-(R)-4,6-O-(E-2-methyl-3-phenyl-2-propenylidene)-β-D-glucopyranoside

There total 4 articles about cyclohexyl 2-acetamido-3-O-benzyl-2-deoxy-(R)-4,6-O-(E-2-methyl-3-phenyl-2-propenylidene)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 100-39-0
benzyl bromide

: 824396-44-3
cyclohexyl 2-acetamido-2-deoxy-(R)-4,6-O-(E-2-methyl-3-phenyl-2-propenylidene)-β-D-glucopyranoside

: 824396-54-5
cyclohexyl 2-acetamido-3-O-benzyl-2-deoxy-(R)-4,6-O-(E-2-methyl-3-phenyl-2-propenylidene)-β-D-glucopyranoside

Guidance literature:: With potassium hydroxide; 18-crown-6 ether; In tetrahydrofuran; at 5 - 20 ℃;
DOI:10.1016/j.tetasy.2004.09.034

Reference yield:

: 21559-72-8
cyclohexyl 2-(acetylamino)-2-deoxy-β-D-glucopyranoside

: 824396-54-5
cyclohexyl 2-acetamido-3-O-benzyl-2-deoxy-(R)-4,6-O-(E-2-methyl-3-phenyl-2-propenylidene)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / anhydrous camphorsulfonic acid / acetonitrile / 20 °C

2: 80 percent / potassium hydroxide; 18-crown-6 / tetrahydrofuran / 5 - 20 °C

With potassium hydroxide; 18-crown-6 ether; camphor-10-sulfonic acid; In tetrahydrofuran; acetonitrile;
DOI:10.1016/j.tetasy.2004.09.034

Reference yield:

: 137032-32-7
α-methyl-trans-cinnamaldehyde dimethyl acetal

: 824396-54-5
cyclohexyl 2-acetamido-3-O-benzyl-2-deoxy-(R)-4,6-O-(E-2-methyl-3-phenyl-2-propenylidene)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / anhydrous camphorsulfonic acid / acetonitrile / 20 °C

2: 80 percent / potassium hydroxide; 18-crown-6 / tetrahydrofuran / 5 - 20 °C

With potassium hydroxide; 18-crown-6 ether; camphor-10-sulfonic acid; In tetrahydrofuran; acetonitrile;
DOI:10.1016/j.tetasy.2004.09.034