Technology Process of C30H41N5O3
There total 7 articles about C30H41N5O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine;
In
1,2-dichloro-ethane;
at 20 ℃;
for 4h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: acetic acid; hydrazine hydrate / ethanol / 0.25 h / 140 °C / Microwave irradiation
1.2: 160 °C
2.1: trifluoroacetic acid / 1,4-dioxane / 20 °C
3.1: bis(tri-t-butylphosphine)palladium (0); N-Methyldicyclohexylamine / 1,4-dioxane / 0.08 h / 130 °C / Microwave irradiation
4.1: diisobutylaluminium hydride / dichloromethane / 3 h / -78 °C
5.1: manganese(IV) oxide / acetonitrile / 2.5 h / 20 °C
6.1: N-ethyl-N,N-diisopropylamine; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 4 h / 20 °C
With
manganese(IV) oxide; bis(tri-t-butylphosphine)palladium (0); N-Methyldicyclohexylamine; sodium tris(acetoxy)borohydride; diisobutylaluminium hydride; hydrazine hydrate; acetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
1,4-dioxane; ethanol; dichloromethane; 1,2-dichloro-ethane; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: potassium 2-methylbutan-2-olate / tetrahydrofuran; toluene / 20 °C
1.2: 0.33 h / 20 °C
2.1: hydrazine hydrate / ethanol / 0.25 h / 140 °C / Microwave irradiation
3.1: trifluoroacetic acid / 1,4-dioxane / 20 °C
4.1: bis(tri-t-butylphosphine)palladium (0); N-Methyldicyclohexylamine / 1,4-dioxane / 0.08 h / 130 °C / Microwave irradiation
5.1: diisobutylaluminium hydride / dichloromethane / 3 h / -78 °C
6.1: manganese(IV) oxide / acetonitrile / 2.5 h / 20 °C
7.1: N-ethyl-N,N-diisopropylamine; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 4 h / 20 °C
With
manganese(IV) oxide; bis(tri-t-butylphosphine)palladium (0); N-Methyldicyclohexylamine; sodium tris(acetoxy)borohydride; diisobutylaluminium hydride; potassium 2-methylbutan-2-olate; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; 1,2-dichloro-ethane; toluene; acetonitrile;