C₂₅H₄₄O₅Si

Base Information

Chemical Name:C₂₅H₄₄O₅Si
CAS No.:1591927-56-8
Molecular Formula:C₂₅H₄₄O₅Si
Molecular Weight:452.707
Hs Code.:

C<sub>25</sub>H<sub>44</sub>O<sub>5</sub>Si

Synonyms:C₂₅H₄₄O₅Si

Suppliers and Price of C₂₅H₄₄O₅Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₅H₄₄O₅Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₅H₄₄O₅Si

There total 10 articles about C₂₅H₄₄O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1591927-94-4
C₁₉H₃₀O₅

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1591927-56-8
C₂₅H₄₄O₅Si

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol5008179

Reference yield:

: 1591927-46-6
C₁₅H₃₄O₂Si₂

: 1591927-56-8
C₂₅H₄₄O₅Si

Guidance literature:: Multi-step reaction with 9 steps

1: boron trifluoride diethyl etherate / dichloromethane / -95 - -78 °C / Inert atmosphere

2: tetramethylammonium triacetoxyborohydride / acetonitrile; acetic acid / 24 h / -40 - -30 °C / Inert atmosphere

3: camphor-10-sulfonic acid / dichloromethane; methanol / 4 h / 0 - 20 °C / Inert atmosphere

4: camphor-10-sulfonic acid / dichloromethane; methanol / 2 h / 0 °C / Inert atmosphere

5: Proton-sponge / dichloromethane / 6 h / 0 - 20 °C / Inert atmosphere

6: diisobutylaluminium hydride / dichloromethane; toluene / -10 °C / Inert atmosphere

7: Dess-Martin periodane / dichloromethane; tert-butyl alcohol / 0 - 20 °C / Inert atmosphere

8: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

9: triethylamine; dmap / dichloromethane / 2 h / 0 °C / Inert atmosphere

With dmap; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; Dess-Martin periodane; triethylamine; tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; methanol; dichloromethane; acetic acid; toluene; acetonitrile; tert-butyl alcohol; 1: |Mukaiyama Aldol Addition;
DOI:10.1021/ol5008179

Reference yield:

: 1591927-49-9
C₃₂H₅₂O₄Si₂

: 1591927-56-8
C₂₅H₄₄O₅Si

Guidance literature:: Multi-step reaction with 8 steps

1: tetramethylammonium triacetoxyborohydride / acetonitrile; acetic acid / 24 h / -40 - -30 °C / Inert atmosphere

2: camphor-10-sulfonic acid / dichloromethane; methanol / 4 h / 0 - 20 °C / Inert atmosphere

3: camphor-10-sulfonic acid / dichloromethane; methanol / 2 h / 0 °C / Inert atmosphere

4: Proton-sponge / dichloromethane / 6 h / 0 - 20 °C / Inert atmosphere

5: diisobutylaluminium hydride / dichloromethane; toluene / -10 °C / Inert atmosphere

6: Dess-Martin periodane / dichloromethane; tert-butyl alcohol / 0 - 20 °C / Inert atmosphere

7: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

8: triethylamine; dmap / dichloromethane / 2 h / 0 °C / Inert atmosphere

With dmap; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; Dess-Martin periodane; triethylamine; tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; methanol; dichloromethane; acetic acid; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1021/ol5008179