C₃₅H₄₀O₆

Base Information

Chemical Name:C₃₅H₄₀O₆
CAS No.:868159-57-3
Molecular Formula:C₃₅H₄₀O₆
Molecular Weight:556.699
Hs Code.:

C<sub>35</sub>H<sub>40</sub>O<sub>6</sub>

Synonyms:C₃₅H₄₀O₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₅H₄₀O₆

Chemical Property:

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Technology Process of C₃₅H₄₀O₆

There total 1 articles about C₃₅H₄₀O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9
2,3,4,6-Tetra-O-benzyl-D-glucopyranose

: 75-16-1
methylmagnesium bromide

: 868159-57-3
C₃₅H₄₀O₆

Guidance literature:: 2,3,4,6-Tetra-O-benzyl-D-glucopyranose; methylmagnesium bromide; In tetrahydrofuran; toluene; at 0 - 50 ℃; for 3.67h; Inert atmosphere;

With ammonium chloride; In tetrahydrofuran; water; toluene;

Reference yield:

: 868159-57-3
C₃₅H₄₀O₆

: 3,4,5,7-tetra-O-benzyl-1-deoxy-D-xylo-hepto-2,6-diulose

Guidance literature:: C₃₅H₄₀O₆; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 - -40 ℃; for 1.25h; Inert atmosphere;

With triethylamine; In dichloromethane; at -78 - 20 ℃; for 2.25h;

Reference yield:

: 868159-57-3
C₃₅H₄₀O₆

: 1413373-28-0
C₅₀H₄₉ClF₂O₅

Guidance literature:: Multi-step reaction with 14 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.25 h / -78 - -40 °C / Inert atmosphere

1.2: 2.25 h / -78 - 20 °C

2.1: L-proline / dimethyl sulfoxide / 8 h / 50 °C

3.1: pyridine; trichlorophosphate / 0 - 20 °C

4.1: cerium(III) chloride heptahydrate / tetrahydrofuran; methanol / 0.5 h / -23 °C

4.2: 0.75 h

5.1: 1H-imidazole / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

5.2: 12 h / 40 °C

6.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

6.2: 2 h / 0 - 20 °C

7.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere

8.1: hydrogenchloride; methanol / dichloromethane / 20 °C

9.1: pyridine / dmap / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

10.1: diethylamino-sulfur trifluoride / dichloromethane / 16 h / 20 °C / Inert atmosphere

11.1: sodium methylate; methanol / 20 °C / Industry scale

12.1: Dess-Martin periodane / dichloromethane / 3 h / 20 °C / Inert atmosphere

12.2: 2 h / 20 °C

13.1: dibromo sulfoxide / dichloromethane / 5 h / -40 - 0 °C / Inert atmosphere

13.2: 1 h / 0 °C

14.1: tri-n-butyl-tin hydride / toluene / 110 °C

With pyridine; 1H-imidazole; hydrogenchloride; methanol; dibromo sulfoxide; oxalyl dichloride; diethylamino-sulfur trifluoride; cerium(III) chloride heptahydrate; dimethylsulfide borane complex; tri-n-butyl-tin hydride; sodium methylate; Dess-Martin periodane; dimethyl sulfoxide; L-proline; trichlorophosphate; dmap; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;