cis-dihydrorose oxide

Base Information

Chemical Name:cis-dihydrorose oxide
CAS No.:140237-69-0
Molecular Formula:C₁₀H₂₀O
Molecular Weight:156.268
Hs Code.:

Synonyms:cis-dihydrorose oxide

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Chemical Property of cis-dihydrorose oxide

Chemical Property:

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Technology Process of cis-dihydrorose oxide

There total 7 articles about cis-dihydrorose oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58303-58-5
2-Isobutyl-4,4-dimethyl-1,3-dioxane

: 140238-78-4
trans-dihydrorose oxide

: 140237-69-0
cis-dihydrorose oxide

: 123-51-3
i-Amyl alcohol

: 63500-71-0,185019-16-3
2-(2-methylpropyl)-4-hydroxy-4-methyl-tetrahydropyran

: 590-86-3
isovaleraldehyde

Guidance literature:: 2-Isobutyl-4,4-dimethyl-1,3-dioxane; at 86 - 92 ℃; for 20h;

With water; hydrogen; at 130 ℃; for 20h; under 7500.75 - 37503.8 Torr; Autoclave; Inert atmosphere;

Reference yield:

: 58303-58-5
2-Isobutyl-4,4-dimethyl-1,3-dioxane

: 140238-78-4
trans-dihydrorose oxide

: 140237-69-0
cis-dihydrorose oxide

: 123-51-3
i-Amyl alcohol

: 63500-71-0,185019-16-3
2-(2-methylpropyl)-4-hydroxy-4-methyl-tetrahydropyran

Guidance literature:: 2-Isobutyl-4,4-dimethyl-1,3-dioxane; at 86 - 92 ℃; for 20h;

With water; hydrogen; at 150 ℃; for 10h; under 7500.75 - 52505.3 Torr; Autoclave; Inert atmosphere;

Reference yield:

: 488-05-1
3-methyl-1-(3-methylfuran-2-yl)butan-1-one

: 5206-80-4,13477-62-8,16665-10-4,91527-21-8,140237-69-0,140237-70-3,140238-78-4,140238-79-5
cis-2-(2-methylpropyl)-4-methyltetrahydropyran

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / LiAlH₄ / diethyl ether / 6 h / 0 °C

2: 3.0 g / H₂ / W-4 Raney nickel / ethanol / 35 - 40 °C / 54340 Torr

3: 56 percent / active alumina / pyridine / 255 °C

4: H₂ / Adam's catalyst / acetic acid

With aluminum oxide; lithium aluminium tetrahydride; hydrogen; platinum(IV) oxide; W-4 Raney nickel; In pyridine; diethyl ether; ethanol; acetic acid;