4',4'''-azoxybis

Base Information

Chemical Name:4',4'''-azoxybis
CAS No.:150195-96-3
Molecular Formula:C₃₈H₄₀Br₂N₂O₅
Molecular Weight:764.554
Hs Code.:

4',4'''-azoxybis<biphenyl-4-carboxylic acid 6-bromohexyl ester>

Synonyms:4',4'''-azoxybis

Suppliers and Price of 4',4'''-azoxybis

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4',4'''-azoxybis

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4',4'''-azoxybis

There total 2 articles about 4',4'''-azoxybis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 4286-55-9
1-bromo-6-hexanol

: 150195-97-4
4',4'''-azoxybis

: 150195-96-3
4',4'''-azoxybis

Guidance literature:: With triethylamine; In 1,2-dichloro-benzene; Ambient temperature;
DOI:10.1002/recl.19931120606

Reference yield:

: 4',4'''-azoxybis

: 150195-96-3
4',4'''-azoxybis

Guidance literature:: Multi-step reaction with 2 steps

1: 20 percent / PCl₅, POCl₃ / 1.) r.t., 4 h, 2.) to 60 deg C

2: 38 percent / Et₃N / 1,2-dichloro-benzene / Ambient temperature

With phosphorus pentachloride; triethylamine; trichlorophosphate; In 1,2-dichloro-benzene;
DOI:10.1002/recl.19931120606