(R)-10-<(N,N-Diisopropylamino)sulfonyl>camphor N-<(1,2-diphenylethyl)sulfonyl>imine

Base Information

Chemical Name:(R)-10-<(N,N-Diisopropylamino)sulfonyl>camphor N-<(1,2-diphenylethyl)sulfonyl>imine
CAS No.:150764-00-4
Molecular Formula:C₃₀H₄₂N₂O₄S₂
Molecular Weight:558.806
Hs Code.:

Synonyms:(R)-10-<(N,N-Diisopropylamino)sulfonyl>camphor N-<(1,2-diphenylethyl)sulfonyl>imine

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Chemical Property of (R)-10-<(N,N-Diisopropylamino)sulfonyl>camphor N-<(1,2-diphenylethyl)sulfonyl>imine

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Technology Process of (R)-10-<(N,N-Diisopropylamino)sulfonyl>camphor N-<(1,2-diphenylethyl)sulfonyl>imine

There total 3 articles about (R)-10-<(N,N-Diisopropylamino)sulfonyl>camphor N-<(1,2-diphenylethyl)sulfonyl>imine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 150763-94-3
(-)-10-<(N,N-Diisopropylamino)sulfonyl>camphor N-(benzylsulfonyl)imine

: 150764-00-4
(R)-10-<(N,N-Diisopropylamino)sulfonyl>camphor N-<(1,2-diphenylethyl)sulfonyl>imine

: (S)-10-<(N,N-Diisopropylamino)sulfonyl>camphor N-<(1,2-diphenylethyl)sulfonyl>imine

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 1h; Yield given. Yields of byproduct given;
DOI:10.1021/jo00070a026

Reference yield:

: 4563-33-1
phenyl-methanesulfonic acid amide

: 150764-00-4
(R)-10-<(N,N-Diisopropylamino)sulfonyl>camphor N-<(1,2-diphenylethyl)sulfonyl>imine

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / TiCl₄ / 1,1,2-trichloro-ethane; CH₂Cl₂ / 16 h / Heating

2: LDA / tetrahydrofuran / 1 h / -78 °C

With titanium tetrachloride; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; 1,1,2-trichloroethane;
DOI:10.1021/jo00070a026

Reference yield:

: 1939-99-7
benzenesulfonyl chloride

: 150764-00-4
(R)-10-<(N,N-Diisopropylamino)sulfonyl>camphor N-<(1,2-diphenylethyl)sulfonyl>imine

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / NH₄OH / CHCl₃

2: 81 percent / TiCl₄ / 1,1,2-trichloro-ethane; CH₂Cl₂ / 16 h / Heating

3: LDA / tetrahydrofuran / 1 h / -78 °C

With ammonium hydroxide; titanium tetrachloride; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; chloroform; 1,1,2-trichloroethane;
DOI:10.1021/jo00070a026