(S)-1-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethanamine

Base Information

Chemical Name:(S)-1-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethanamine
CAS No.:1260955-16-5
Molecular Formula:C₁₄H₂₂BNO₂
Molecular Weight:247.145
Hs Code.:

Synonyms:(S)-1-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-1-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethanamine

Chemical Property:

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Technology Process of (S)-1-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethanamine

There total 3 articles about (S)-1-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 214360-49-3
1-[3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethanone

: 1260955-16-5
(S)-1-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethanamine

Guidance literature:: With Candida boidinii formate dehydrogenase; 2-aminopropanoic acid; alanine dehydrogenase; pyridoxal 5'-phosphate; Chromobacterium violaceum ω-transaminase; ammonium formate; NADP; In aq. phosphate buffer; dimethyl sulfoxide; at 30 ℃; for 24h; Enzymatic reaction;
DOI:10.1016/j.tetasy.2013.10.004

Reference yield:

: 76-09-5
2,3-dimethyl-2,3-butane diol

: C₈H₁₂BNO₂

: 1260955-16-5
(S)-1-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethanamine

Guidance literature:: In tetrahydrofuran; Heating;
DOI:10.1016/j.tetasy.2013.10.004

Reference yield:

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 1260955-16-5
(S)-1-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 40 °C

2: 2-aminopropanoic acid; pyridoxal 5'-phosphate; NADP; ammonium formate; Candida boidinii formate dehydrogenase; alanine dehydrogenase; Chromobacterium violaceum ω-transaminase / aq. phosphate buffer; dimethyl sulfoxide / 24 h / 30 °C / Enzymatic reaction

With Candida boidinii formate dehydrogenase; 2-aminopropanoic acid; alanine dehydrogenase; pyridoxal 5'-phosphate; Chromobacterium violaceum ω-transaminase; ammonium formate; NADP; In tetrahydrofuran; aq. phosphate buffer; dimethyl sulfoxide;
DOI:10.1016/j.tetasy.2013.10.004