methyl 2,3-di-O-benzyl-6-O-propionyl-1-thio-4-O-tosyl-β-D-galactopyranoside

Base Information

Chemical Name:methyl 2,3-di-O-benzyl-6-O-propionyl-1-thio-4-O-tosyl-β-D-galactopyranoside
CAS No.:122079-67-8
Molecular Formula:C₃₁H₃₆O₈S₂
Molecular Weight:600.754
Hs Code.:

Synonyms:methyl 2,3-di-O-benzyl-6-O-propionyl-1-thio-4-O-tosyl-β-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2,3-di-O-benzyl-6-O-propionyl-1-thio-4-O-tosyl-β-D-galactopyranoside

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Technology Process of methyl 2,3-di-O-benzyl-6-O-propionyl-1-thio-4-O-tosyl-β-D-galactopyranoside

There total 5 articles about methyl 2,3-di-O-benzyl-6-O-propionyl-1-thio-4-O-tosyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 122079-65-6
methyl 2,3-di-O-benzyl-6-O-propionyl-1-thio-β-D-galactopyranoside

: 98-59-9
p-toluenesulfonyl chloride

: 122079-67-8
methyl 2,3-di-O-benzyl-6-O-propionyl-1-thio-4-O-tosyl-β-D-galactopyranoside

Guidance literature:: With pyridine; dmap; 1 day, room t., then 4 days, 60 deg C;
DOI:10.1016/0008-6215(89)84037-6

Reference yield:

: 100-39-0
benzyl bromide

: 122079-67-8
methyl 2,3-di-O-benzyl-6-O-propionyl-1-thio-4-O-tosyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) DMF, 2.) DMF, 0 deg C, then 3 h, room t.

2: 92 percent / aq. 60percent AcOH / 0.5 h / Heating

3: 70 percent / pyridine / 0 deg C, 8 h, then room t., 1 day

4: 85 percent / pyridine, DMAP / 1 day, room t., then 4 days, 60 deg C

With pyridine; dmap; sodium hydride; acetic acid;
DOI:10.1016/0008-6215(89)84037-6

Reference yield:

: 122079-64-5
methyl 2,3-di-O-benzyl-1-thio-β-D-galactopyranoside

: 122079-67-8
methyl 2,3-di-O-benzyl-6-O-propionyl-1-thio-4-O-tosyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / pyridine / 0 deg C, 8 h, then room t., 1 day

2: 85 percent / pyridine, DMAP / 1 day, room t., then 4 days, 60 deg C

With pyridine; dmap;
DOI:10.1016/0008-6215(89)84037-6