1-({1-[(1-methoxycyclododecyl)peroxy]cyclohexyl}peroxy)cyclohexyl hydroperoxide

Base Information

• Chemical Name: 1-({1-[(1-methoxycyclododecyl)peroxy]cyclohexyl}peroxy)cyclohexyl hydroperoxide
• CAS No.: 952311-36-3
• Molecular Formula: C₂₅H₄₆O₇
• Molecular Weight: 458.636
• Mol file: 952311-36-3.mol

Synonyms:1-({1-[(1-methoxycyclododecyl)peroxy]cyclohexyl}peroxy)cyclohexyl hydroperoxide

Chemical Property of 1-({1-[(1-methoxycyclododecyl)peroxy]cyclohexyl}peroxy)cyclohexyl hydroperoxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-({1-[(1-methoxycyclododecyl)peroxy]cyclohexyl}peroxy)cyclohexyl hydroperoxide

There total 2 articles about 1-({1-[(1-methoxycyclododecyl)peroxy]cyclohexyl}peroxy)cyclohexyl hydroperoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

bis-(1-hydroperoxycyclohexyl)peroxide (2699-12-9) + Cyclododecanone dimethoxy acetal (950-33-4) → 1-({1-[(1-methoxycyclododecyl)peroxy]cyclohexyl}peroxy)cyclohexyl hydroperoxide (952311-36-3)

Guidance literature:

With boron trifluoride diethyl etherate; In diethyl ether; at 20 - 25 ℃; for 0.5h;

DOI:10.1021/jo071072c

Reference yield:

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → 1-({1-[(1-methoxycyclododecyl)peroxy]cyclohexyl}peroxy)cyclohexyl hydroperoxide (952311-36-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 63 percent / aq. H₂O₂; H₂SO₄ / 1 h / 10 - 15 °C

2: 14 percent / BF₃*Et₂O / diethyl ether / 0.5 h / 20 - 25 °C

With sulfuric acid; boron trifluoride diethyl etherate; dihydrogen peroxide; In diethyl ether;

DOI:10.1021/jo071072c

upstream raw materials:

bis-(1-hydroperoxycyclohexyl)peroxide

Cyclododecanone dimethoxy acetal

cyclohexanone