N₂,N₂-dibenzyl-6-bromo-N₄-(6-methyl-pyridin-3-ylmethyl)-3-nitropyridine-2,4-diamine

Base Information

• Chemical Name: N₂,N₂-dibenzyl-6-bromo-N₄-(6-methyl-pyridin-3-ylmethyl)-3-nitropyridine-2,4-diamine
• CAS No.: 947146-11-4
• Molecular Formula: C₂₆H₂₄BrN₅O₂
• Molecular Weight: 518.413

Synonyms:N₂,N₂-dibenzyl-6-bromo-N₄-(6-methyl-pyridin-3-ylmethyl)-3-nitropyridine-2,4-diamine

Chemical Property of N₂,N₂-dibenzyl-6-bromo-N₄-(6-methyl-pyridin-3-ylmethyl)-3-nitropyridine-2,4-diamine

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Technology Process of N₂,N₂-dibenzyl-6-bromo-N₄-(6-methyl-pyridin-3-ylmethyl)-3-nitropyridine-2,4-diamine

There total 1 articles about N₂,N₂-dibenzyl-6-bromo-N₄-(6-methyl-pyridin-3-ylmethyl)-3-nitropyridine-2,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-(bromomethyl)-2-methylpyridine (792187-67-8) + N2,N2-dibenzyl-6-bromo-3-nitro-pyridine-2,4-diamine (947146-08-9) → N2,N2-dibenzyl-6-bromo-N4-(6-methyl-pyridin-3-ylmethyl)-3-nitropyridine-2,4-diamine (947146-11-4)

Guidance literature:

N₂,N₂-dibenzyl-6-bromo-3-nitro-pyridine-2,4-diamine; With potassium tert-butylate; In tetrahydrofuran; at -18 ℃; for 0.0833333h; Cooling with ice/salt bath;

5-(bromomethyl)-2-methylpyridine; In tetrahydrofuran; 2-methyltetrahydrofuran; at -18 - 20 ℃; for 48h; Cooling with ice/salt bath;

With potassium tert-butylate; tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; 2-methyltetrahydrofuran; at -18 - 20 ℃; for 4h; Cooling with ice/salt bath;

Reference yield:

oxazol (288-42-6) + N2,N2-dibenzyl-6-bromo-N4-(6-methyl-pyridin-3-ylmethyl)-3-nitropyridine-2,4-diamine (947146-11-4) → N2,N2-Dibenzyl-N4-(6-methyl-pyridin-3-ylmethyl)-3-nitro-6-oxazol-2-yl-pyridine-2,4-diamine (947146-15-8)

Guidance literature:

oxazol; With n-butyllithium; In tetrahydrofuran; at -78 - -60 ℃; for 0.166667h; Cooling with acetone-dry ice;

With zinc(II) chloride; In tetrahydrofuran; at -78 - 20 ℃;

N₂,N₂-dibenzyl-6-bromo-N₄-(6-methyl-pyridin-3-ylmethyl)-3-nitropyridine-2,4-diamine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; at 130 ℃; for 0.25h; Microwave irradiation;

upstream raw materials:

5-(bromomethyl)-2-methylpyridine

N₂,N₂-dibenzyl-6-bromo-3-nitro-pyridine-2,4-diamine

Downstream raw materials:

N₂,N₂-Dibenzyl-N₄-(6-methyl-pyridin-3-ylmethyl)-3-nitro-6-oxazol-2-yl-pyridine-2,4-diamine

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