(R)-2-((R)-2-Methylene-cyclopentyl)-propionic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

Base Information

• Chemical Name: (R)-2-((R)-2-Methylene-cyclopentyl)-propionic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester
• CAS No.: 173937-31-0
• Molecular Formula: C₂₅H₃₆O₂
• Molecular Weight: 368.56

Synonyms:(R)-2-((R)-2-Methylene-cyclopentyl)-propionic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

Chemical Property of (R)-2-((R)-2-Methylene-cyclopentyl)-propionic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

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Technology Process of (R)-2-((R)-2-Methylene-cyclopentyl)-propionic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

There total 2 articles about (R)-2-((R)-2-Methylene-cyclopentyl)-propionic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

((R)-2-Methylene-cyclopentyl)-acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester + methyl iodide (74-88-4) → (R)-2-((R)-2-Methylene-cyclopentyl)-propionic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester (173937-31-0)

Guidance literature:

With lithium cyclohexylisopropylamide; In tetrahydrofuran; at -78 ℃;

DOI:10.1016/0957-4166(95)00350-X

Reference yield:

(-)-8-phenylmenthyl 2-methyl-2-octene-7-ynoate → (R)-2-((S)-2-Methylene-cyclopentyl)-propionic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester + (R)-2-((R)-2-Methylene-cyclopentyl)-propionic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester (173937-31-0) + (S)-2-((S)-2-Methylene-cyclopentyl)-propionic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester + (S)-2-((R)-2-Methylene-cyclopentyl)-propionic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; at 80 ℃; Product distribution; Mechanism; other substrate, also in the presence of Et₃B instead AIBN; var. temp.; other solvents;

DOI:10.1016/0957-4166(95)00350-X

Reference yield:

(R)-2-((R)-2-Methylene-cyclopentyl)-propionic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester (173937-31-0) → (S)-2-((R)-2-Methylene-cyclopentyl)-propionic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

Guidance literature:

With lithium cyclohexylisopropylamide; isopropyl alcohol; Yield given. Multistep reaction; 1.) THF, 2.) THF, -78 deg C;

DOI:10.1016/0957-4166(95)00350-X

upstream raw materials:

methyl iodide

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