methyl 2-((1-(4-(N-phenethylsulfamoyl)phenyl)-1H-1,2,3-triazol-4-yl)methoxy)benzoate

Base Information

Chemical Name:methyl 2-((1-(4-(N-phenethylsulfamoyl)phenyl)-1H-1,2,3-triazol-4-yl)methoxy)benzoate
CAS No.:1456736-85-8
Molecular Formula:C₂₅H₂₄N₄O₅S
Molecular Weight:492.555
Hs Code.:

Synonyms:methyl 2-((1-(4-(N-phenethylsulfamoyl)phenyl)-1H-1,2,3-triazol-4-yl)methoxy)benzoate

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Chemical Property of methyl 2-((1-(4-(N-phenethylsulfamoyl)phenyl)-1H-1,2,3-triazol-4-yl)methoxy)benzoate

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Technology Process of methyl 2-((1-(4-(N-phenethylsulfamoyl)phenyl)-1H-1,2,3-triazol-4-yl)methoxy)benzoate

There total 5 articles about methyl 2-((1-(4-(N-phenethylsulfamoyl)phenyl)-1H-1,2,3-triazol-4-yl)methoxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 59155-84-9
methyl 2-(prop-2-yn-1-yloxy)benzoate

: 1456736-75-6
4-azido-N-phenethylbenzenesulfonamide

: 1456736-85-8
methyl 2-((1-(4-(N-phenethylsulfamoyl)phenyl)-1H-1,2,3-triazol-4-yl)methoxy)benzoate

Guidance literature:: With Vitamin C; copper(II) sulfate pentahydrate; In water; tert-butyl alcohol; at 20 ℃; for 2h;
DOI:10.1007/s00044-013-0777-z

Reference yield:

: 64-04-0
phenethylamine

: 1456736-85-8
methyl 2-((1-(4-(N-phenethylsulfamoyl)phenyl)-1H-1,2,3-triazol-4-yl)methoxy)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium carbonate

2.1: tin(II) chloride dihdyrate / ethanol / 4 h / Reflux

3.1: hydrogenchloride; acetic acid; sodium nitrite / water / 0.25 h / 0 °C

3.2: 0.5 h / 50 °C

4.1: copper(II) sulfate pentahydrate; Vitamin C / water; tert-butyl alcohol / 2 h / 20 °C

With hydrogenchloride; tin(II) chloride dihdyrate; Vitamin C; copper(II) sulfate pentahydrate; sodium carbonate; acetic acid; sodium nitrite; In ethanol; water; tert-butyl alcohol;
DOI:10.1007/s00044-013-0777-z

Reference yield:

: 587850-67-7
4-amino-N-phenethyl-benzenesulfonamide

: 1456736-85-8
methyl 2-((1-(4-(N-phenethylsulfamoyl)phenyl)-1H-1,2,3-triazol-4-yl)methoxy)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; acetic acid; sodium nitrite / water / 0.25 h / 0 °C

1.2: 0.5 h / 50 °C

2.1: copper(II) sulfate pentahydrate; Vitamin C / water; tert-butyl alcohol / 2 h / 20 °C

With hydrogenchloride; Vitamin C; copper(II) sulfate pentahydrate; acetic acid; sodium nitrite; In water; tert-butyl alcohol;
DOI:10.1007/s00044-013-0777-z