{Ir(OC₆H₅)COD}2

Base Information

Chemical Name:{Ir(OC₆H₅)COD}2
CAS No.:35429-67-5
Molecular Formula:C₂₈H₃₄Ir₂O₂
Molecular Weight:787.017
Hs Code.:

Synonyms:{Ir(OC₆H₅)COD}2

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Chemical Property of {Ir(OC₆H₅)COD}2

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Technology Process of {Ir(OC₆H₅)COD}2

There total 1 articles about {Ir(OC₆H₅)COD}2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: chloro(1,5-cyclooctadiene)iridium(I) dimer

: 108-95-2,27073-41-2
phenol

: 35429-67-5
{Ir(OC₆H₅)COD}2

Guidance literature:: With KOH; In dichloromethane; byproducts: KCl; addn. of mixture of KOH and phenol in CH2Cl2 to soln. of (IrClCOD)2, stirring resulting slurry for 2 h, all operations under inert atmosphere; collection of resulting solid on a Schlenk frit, washing with water (4 times), drying in vacuo ; elem. anal.;
DOI:10.1021/om00105a013

Reference yield: 100.0%

: 35429-67-5
{Ir(OC₆H₅)COD}2

: 34989-06-5
Bis<3-(diphenylphosphino)propyl>phenylphosphin

: 118657-67-3
Ir(OC₆H₅)(ttp)

: 5259-72-3,10060-40-9,111-78-4
cyclo-octa-1,5-diene

Guidance literature:: In toluene; addn. of soln. of ttp to suspension of Ir-complex, stirring a few mins. (formation of clear soln.), refluxing 18 h, cooling to room temp; all operations under inert atmosphere; evapn., addn. of hexane, pptn., collection of solid on a Schlenk frit, washing with hexane (3 times), drying in vacuo; elem. anal.;
DOI:10.1021/om00105a013

Reference yield: 47.0%

: 35429-67-5
{Ir(μ-OPh)(cod)}2

: 2622-14-2
tricyclohexylphosphine

: 119694-76-7
Ir(OPh)(cod)(PCy₃)

Guidance literature:: In diethyl ether; stirring (Ir(μ-OPh)(cod))2 and PCy3 in diethylether (room temp., 5 h, N2), pptn.; concg., adding acetone, pptn., filtering, washing (acetone), drying (vacuum); elem. anal.;