(6R,7R,7aR)-7-(benzyloxy)-7a-(hydroxymethyl)-6-methyltetrahydropyrrolo[1,2-c]oxazol-3(1H)-one

Base Information

Chemical Name:(6R,7R,7aR)-7-(benzyloxy)-7a-(hydroxymethyl)-6-methyltetrahydropyrrolo[1,2-c]oxazol-3(1H)-one
CAS No.:1257304-40-7
Molecular Formula:C₁₅H₁₉NO₄
Molecular Weight:277.32
Hs Code.:

Synonyms:(6R,7R,7aR)-7-(benzyloxy)-7a-(hydroxymethyl)-6-methyltetrahydropyrrolo[1,2-c]oxazol-3(1H)-one

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Chemical Property of (6R,7R,7aR)-7-(benzyloxy)-7a-(hydroxymethyl)-6-methyltetrahydropyrrolo[1,2-c]oxazol-3(1H)-one

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Technology Process of (6R,7R,7aR)-7-(benzyloxy)-7a-(hydroxymethyl)-6-methyltetrahydropyrrolo[1,2-c]oxazol-3(1H)-one

There total 2 articles about (6R,7R,7aR)-7-(benzyloxy)-7a-(hydroxymethyl)-6-methyltetrahydropyrrolo[1,2-c]oxazol-3(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1257304-47-4
C₁₈H₂₅NO₄

: 1257304-40-7
(6R,7R,7aR)-7-(benzyloxy)-7a-(hydroxymethyl)-6-methyltetrahydropyrrolo[1,2-c]oxazol-3(1H)-one

Guidance literature:: formaldehyd; C₁₈H₂₅NO₄; With sodium hydroxide; In water; at 20 ℃; for 96h;

With sodium hydroxide; In tetrahydrofuran; methanol; water; at 20 ℃; for 4h;
DOI:10.1055/s-0030-1257872

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1257304-47-4
C₁₈H₂₅NO₄

: 1257304-40-7
(6R,7R,7aR)-7-(benzyloxy)-7a-(hydroxymethyl)-6-methyltetrahydropyrrolo[1,2-c]oxazol-3(1H)-one

: 1257304-48-5
C₁₉H₂₉NO₅

Guidance literature:: With sodium hydroxide; In water; at 20 ℃; for 96h;
DOI:10.1055/s-0030-1257872

Reference yield: 92.0%

: 1257304-40-7
(6R,7R,7aR)-7-(benzyloxy)-7a-(hydroxymethyl)-6-methyltetrahydropyrrolo[1,2-c]oxazol-3(1H)-one

: 1257304-49-6
C₁₅H₁₇NO₄

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 - 20 ℃;
DOI:10.1055/s-0030-1257872