phenylmethyl 3-deoxy-3-[4-(1,1-dimethylethoxy)-2,4-dioxobutyl]-4-O-(methoxymethyl)-β-L-xylopyranoside

Base Information

Chemical Name:phenylmethyl 3-deoxy-3-[4-(1,1-dimethylethoxy)-2,4-dioxobutyl]-4-O-(methoxymethyl)-β-L-xylopyranoside
CAS No.:162332-28-7
Molecular Formula:C₂₂H₃₂O₈
Molecular Weight:424.491
Hs Code.:

Synonyms:phenylmethyl 3-deoxy-3-[4-(1,1-dimethylethoxy)-2,4-dioxobutyl]-4-O-(methoxymethyl)-β-L-xylopyranoside

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Chemical Property of phenylmethyl 3-deoxy-3-[4-(1,1-dimethylethoxy)-2,4-dioxobutyl]-4-O-(methoxymethyl)-β-L-xylopyranoside

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Technology Process of phenylmethyl 3-deoxy-3-[4-(1,1-dimethylethoxy)-2,4-dioxobutyl]-4-O-(methoxymethyl)-β-L-xylopyranoside

There total 1 articles about phenylmethyl 3-deoxy-3-[4-(1,1-dimethylethoxy)-2,4-dioxobutyl]-4-O-(methoxymethyl)-β-L-xylopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1694-31-1
tert-butyl acetoacetate

: benzyl 2,3-anhydro-4-O-methoxymethyl-β-L-ribopyranoside

: 162332-28-7
phenylmethyl 3-deoxy-3-[4-(1,1-dimethylethoxy)-2,4-dioxobutyl]-4-O-(methoxymethyl)-β-L-xylopyranoside

Guidance literature:: tert-butyl acetoacetate; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.75h; Inert atmosphere;

With n-butyllithium; In tetrahydrofuran; hexane; mineral oil; at 0 ℃; for 0.666667h; Inert atmosphere;

benzyl 2,3-anhydro-4-O-methoxymethyl-β-L-ribopyranoside; In tetrahydrofuran; hexane; mineral oil; at 0 - 20 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1021/jo900192a