C₂₉H₅₀O₅Si

Base Information

Chemical Name:C₂₉H₅₀O₅Si
CAS No.:881035-45-6
Molecular Formula:C₂₉H₅₀O₅Si
Molecular Weight:506.798
Hs Code.:

C<sub>29</sub>H<sub>50</sub>O<sub>5</sub>Si

Synonyms:C₂₉H₅₀O₅Si

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Chemical Property of C₂₉H₅₀O₅Si

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Technology Process of C₂₉H₅₀O₅Si

There total 11 articles about C₂₉H₅₀O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 881035-27-4
C₂₈H₄₈O₆Si

: 1779-49-3
Methyltriphenylphosphonium bromide

: 881035-45-6
C₂₉H₅₀O₅Si

Guidance literature:: Methyltriphenylphosphonium bromide; With sodium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃; for 1h;

C₂₈H₄₈O₆Si; In tetrahydrofuran; at 0 ℃; for 0.5h; Further stages.;
DOI:10.1039/b517385j

Reference yield:

: 881035-25-2
C₂₀H₃₅BrO₅Si

: 881035-45-6
C₂₉H₅₀O₅Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: 85 percent / n-Bu₃SnOMe; (2'-diphenylphosphanyl-biphenyl-2-yl)-dimethyl-amine / Pd₂(dba)3 / toluene / 2 h / 90 °C

2.1: NaH / tetrahydrofuran / 0.5 h / 0 °C

2.2: 73 percent / tetrahydrofuran / 4 h / 0 °C

3.1: NaHMDS / tetrahydrofuran / 1 h / 0 °C

3.2: 75 percent / tetrahydrofuran / 0.5 h / 0 °C

With tributyltin methoxide; sodium hexamethyldisilazane; sodium hydride; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In tetrahydrofuran; toluene; 3.2: Wittig reaction;
DOI:10.1039/b517385j

Reference yield:

: 881035-24-1
C₉H₉BrO₄

: 881035-45-6
C₂₉H₅₀O₅Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: 85 percent / NaH / dimethylformamide / 2 h / 25 °C

2.1: 90 percent / NaBH₄ / methanol / 0.5 h / 0 °C

3.1: 85 percent / imidazole; 4-DMAP / dimethylformamide / 12 h / 25 °C

4.1: 85 percent / n-Bu₃SnOMe; (2'-diphenylphosphanyl-biphenyl-2-yl)-dimethyl-amine / Pd₂(dba)3 / toluene / 2 h / 90 °C

5.1: NaH / tetrahydrofuran / 0.5 h / 0 °C

5.2: 73 percent / tetrahydrofuran / 4 h / 0 °C

6.1: NaHMDS / tetrahydrofuran / 1 h / 0 °C

6.2: 75 percent / tetrahydrofuran / 0.5 h / 0 °C

With 1H-imidazole; dmap; sodium tetrahydroborate; tributyltin methoxide; sodium hexamethyldisilazane; sodium hydride; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene; 6.2: Wittig reaction;
DOI:10.1039/b517385j