C₃₆H₃₁N₃O₅

Base Information

Chemical Name:C₃₆H₃₁N₃O₅
CAS No.:188028-28-6
Molecular Formula:C₃₆H₃₁N₃O₅
Molecular Weight:585.659
Hs Code.:

C<sub>36</sub>H<sub>31</sub>N<sub>3</sub>O<sub>5</sub>

Synonyms:C₃₆H₃₁N₃O₅

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Chemical Property of C₃₆H₃₁N₃O₅

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Technology Process of C₃₆H₃₁N₃O₅

There total 7 articles about C₃₆H₃₁N₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 188027-96-5
C₃₆H₃₃N₃O₆

: 188028-28-6
C₃₆H₃₁N₃O₅

Guidance literature:: With Martins sulfurane; In chloroform-d1; for 0.333333h;
DOI:10.1021/ja971304x

Reference yield:

: 188027-92-1
C₃₅H₃₁N₃O₆

: 188028-28-6
C₃₆H₃₁N₃O₅

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1) THF, 25 min; 2) THF, 50 min

2: 88 percent / Martin's sulfurane / CDCl₃ / 0.33 h

With Martins sulfurane; sodium hydride; In chloroform-d1;
DOI:10.1021/ja971304x

Reference yield:

: 188028-23-1
C₃₅H₃₁N₃O₆

: 188028-28-6
C₃₆H₃₁N₃O₅

Guidance literature:: Multi-step reaction with 5 steps

1: 71 percent / pyridinium trifluoroacetate, 1,3-dicyclohexylcarbodiimide / benzene; dimethylsulfoxide / 9 h / Ambient temperature

2: 85 percent / BF₃*OEt₂ / diethyl ether / 24 h / 25 - 30 °C

3: 95 percent / NaBH₄ / methanol; CH₂Cl₂; CHCl₃ / 0.08 h

4: 1.) NaH / 1) THF, 25 min; 2) THF, 50 min

5: 88 percent / Martin's sulfurane / CDCl₃ / 0.33 h

With sodium tetrahydroborate; Martins sulfurane; boron trifluoride diethyl etherate; pyridinium trifluroacetate; sodium hydride; dicyclohexyl-carbodiimide; In methanol; diethyl ether; chloroform-d1; dichloromethane; chloroform; dimethyl sulfoxide; benzene;
DOI:10.1021/ja971304x