tert-Butyl (3S,4S,5S)-3-methoxy-4--5-methylheptanoate

Base Information

Chemical Name:tert-Butyl (3S,4S,5S)-3-methoxy-4--5-methylheptanoate
CAS No.:154633-73-5
Molecular Formula:C₂₂H₃₅NO₅
Molecular Weight:393.524
Hs Code.:

tert-Butyl (3S,4S,5S)-3-methoxy-4-<N-(benzyloxycarbonyl)-N-methylamino>-5-methylheptanoate

Synonyms:tert-Butyl (3S,4S,5S)-3-methoxy-4--5-methylheptanoate

Suppliers and Price of tert-Butyl (3S,4S,5S)-3-methoxy-4--5-methylheptanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of tert-Butyl (3S,4S,5S)-3-methoxy-4--5-methylheptanoate

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of tert-Butyl (3S,4S,5S)-3-methoxy-4--5-methylheptanoate

There total 8 articles about tert-Butyl (3S,4S,5S)-3-methoxy-4--5-methylheptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 420-37-1
trimethoxonium tetrafluoroborate

: 120205-57-4
tert-Butyl (3S,4S,5S)-3-hydroxy-4--5-methylheptanoate

tert-Butyl (3S,4S,5S)-3-methoxy-4--5-methylheptanoate: 154633-73-5
tert-Butyl (3S,4S,5S)-3-methoxy-4--5-methylheptanoate

Guidance literature:: With 4 A molecular sieve; In 1,2-dichloro-ethane; for 20h; Ambient temperature;
DOI:10.1021/jo00086a034

Reference yield: 67.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 120205-57-4
tert-Butyl (3S,4S,5S)-3-hydroxy-4--5-methylheptanoate

tert-Butyl (3S,4S,5S)-3-methoxy-4--5-methylheptanoate: 154633-73-5
tert-Butyl (3S,4S,5S)-3-methoxy-4--5-methylheptanoate

Guidance literature:: With boron trifluoride diethyl etherate;
DOI:10.1021/ja00196a061

Reference yield:

: 540-88-5
acetic acid tert-butyl ester

tert-Butyl (3S,4S,5S)-3-methoxy-4--5-methylheptanoate: 154633-73-5
tert-Butyl (3S,4S,5S)-3-methoxy-4--5-methylheptanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.)lithium diisopropylamide / 2.) THF, -78 deg C, 45 min

2: 67 percent / BF₃*Et₂O

With boron trifluoride diethyl etherate; lithium diisopropyl amide;
DOI:10.1021/ja00196a061