(1R)-camphor-2-(1-methanesulfonyl)glycerol-spiro-ketal-10-sulfonyldibenzylamine

Base Information

Chemical Name:(1R)-camphor-2-(1-methanesulfonyl)glycerol-spiro-ketal-10-sulfonyldibenzylamine
CAS No.:251929-32-5
Molecular Formula:C₂₈H₃₇NO₇S₂
Molecular Weight:563.736
Hs Code.:

Synonyms:(1R)-camphor-2-(1-methanesulfonyl)glycerol-spiro-ketal-10-sulfonyldibenzylamine

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Chemical Property of (1R)-camphor-2-(1-methanesulfonyl)glycerol-spiro-ketal-10-sulfonyldibenzylamine

Chemical Property:

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Technology Process of (1R)-camphor-2-(1-methanesulfonyl)glycerol-spiro-ketal-10-sulfonyldibenzylamine

There total 4 articles about (1R)-camphor-2-(1-methanesulfonyl)glycerol-spiro-ketal-10-sulfonyldibenzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 124-63-0
methanesulfonyl chloride

: 251929-31-4
(1R)-camphor-2-glycerol-spiro-ketal-10-sulfonyldibenzylamine

: 251929-32-5
(1R)-camphor-2-(1-methanesulfonyl)glycerol-spiro-ketal-10-sulfonyldibenzylamine

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1021/jo000503n

Reference yield:

: 21286-54-4,39262-22-1
D-camphor-10-sulfonyl chloride

: 251929-32-5
(1R)-camphor-2-(1-methanesulfonyl)glycerol-spiro-ketal-10-sulfonyldibenzylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / DMAP / CH₂Cl₂ / 1 h / 0 °C

2: 43 percent / p-toluenesulfonic acid monohydrate / toluene / 3 h / Heating

3: 95 percent / triethylamine / CH₂Cl₂ / 3 h / 20 °C

With dmap; toluene-4-sulfonic acid; triethylamine; In dichloromethane; toluene; 1: Substitution / 2: cyclocondensation / 3: mesylation;
DOI:10.1021/jo000503n

Reference yield:

: 251929-30-3,616214-72-3
(1R)-camphor-10-sulfonyldibenzylamine

: 251929-32-5
(1R)-camphor-2-(1-methanesulfonyl)glycerol-spiro-ketal-10-sulfonyldibenzylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / p-toluenesulfonic acid monohydrate / toluene / 3 h / Heating

2: 95 percent / triethylamine / CH₂Cl₂ / 3 h / 20 °C

With toluene-4-sulfonic acid; triethylamine; In dichloromethane; toluene; 1: cyclocondensation / 2: mesylation;
DOI:10.1021/jo000503n