di-tert-butyl 1,2-bis(2-(5-methoxy-1-tosyl-indol-3-yl)ethyl)hydrazine-1,2-dicarboxylate

Base Information

Chemical Name:di-tert-butyl 1,2-bis(2-(5-methoxy-1-tosyl-indol-3-yl)ethyl)hydrazine-1,2-dicarboxylate
CAS No.:1453190-46-9
Molecular Formula:C₄₆H₅₄N₄O₁₀S₂
Molecular Weight:887.088
Hs Code.:

Synonyms:di-tert-butyl 1,2-bis(2-(5-methoxy-1-tosyl-indol-3-yl)ethyl)hydrazine-1,2-dicarboxylate

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Chemical Property of di-tert-butyl 1,2-bis(2-(5-methoxy-1-tosyl-indol-3-yl)ethyl)hydrazine-1,2-dicarboxylate

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Technology Process of di-tert-butyl 1,2-bis(2-(5-methoxy-1-tosyl-indol-3-yl)ethyl)hydrazine-1,2-dicarboxylate

There total 3 articles about di-tert-butyl 1,2-bis(2-(5-methoxy-1-tosyl-indol-3-yl)ethyl)hydrazine-1,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1026250-24-7
2-(5-methoxy-1-tosyl-1H-indol-3-yl)ethyl 4-methylbenzenesulfonate

: 16466-61-8
1,2-bis(t-butyloxycarbonyl)hydrazine

: 1453190-46-9
di-tert-butyl 1,2-bis(2-(5-methoxy-1-tosyl-indol-3-yl)ethyl)hydrazine-1,2-dicarboxylate

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 120h; Inert atmosphere;
DOI:10.1016/j.tetlet.2013.07.134

Reference yield:

: 19501-58-7
4-methoxyphenylhydrazine hydrochloride

: 1453190-46-9
di-tert-butyl 1,2-bis(2-(5-methoxy-1-tosyl-indol-3-yl)ethyl)hydrazine-1,2-dicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid / N,N-dimethyl acetamide / 2 h / 55 °C

2.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C / Cooling with ice; Inert atmosphere

2.2: 18.17 h / 0 - 20 °C

3.1: caesium carbonate / N,N-dimethyl-formamide / 120 h / 20 °C / Inert atmosphere

With sulfuric acid; sodium hydride; caesium carbonate; In tetrahydrofuran; N,N-dimethyl acetamide; N,N-dimethyl-formamide; 1.1: |Fischer Indole Synthesis;
DOI:10.1016/j.tetlet.2013.07.134

Reference yield:

: 712-09-4
5-methoxytryptophol

: 1453190-46-9
di-tert-butyl 1,2-bis(2-(5-methoxy-1-tosyl-indol-3-yl)ethyl)hydrazine-1,2-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C / Cooling with ice; Inert atmosphere

1.2: 18.17 h / 0 - 20 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 120 h / 20 °C / Inert atmosphere

With sodium hydride; caesium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2013.07.134