3-(4-methoxy-3-methylsulfanyl-5-trifluoromethylbenzoyl)-2,3-dihydro-1,3-benzothiazole

Base Information

Chemical Name:3-(4-methoxy-3-methylsulfanyl-5-trifluoromethylbenzoyl)-2,3-dihydro-1,3-benzothiazole
CAS No.:1285575-26-9
Molecular Formula:C₁₇H₁₄F₃NO₂S₂
Molecular Weight:385.431
Hs Code.:

Synonyms:3-(4-methoxy-3-methylsulfanyl-5-trifluoromethylbenzoyl)-2,3-dihydro-1,3-benzothiazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(4-methoxy-3-methylsulfanyl-5-trifluoromethylbenzoyl)-2,3-dihydro-1,3-benzothiazole

Chemical Property:

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Technology Process of 3-(4-methoxy-3-methylsulfanyl-5-trifluoromethylbenzoyl)-2,3-dihydro-1,3-benzothiazole

There total 12 articles about 3-(4-methoxy-3-methylsulfanyl-5-trifluoromethylbenzoyl)-2,3-dihydro-1,3-benzothiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4433-52-7
2,3-dihydro-benzothiazole

: 1285575-24-7
4-methoxy-3-methylsulfanyl-5-trifluoromethylbenzoyl chloride

: 1285575-26-9
3-(4-methoxy-3-methylsulfanyl-5-trifluoromethylbenzoyl)-2,3-dihydro-1,3-benzothiazole

Guidance literature:: With triethylamine; In chloroform; at 20 ℃; for 1h;

Reference yield:

: 115933-50-1
methyl 4-hydroxy-3-(trifluoromethyl)benzoate

: 1285575-26-9
3-(4-methoxy-3-methylsulfanyl-5-trifluoromethylbenzoyl)-2,3-dihydro-1,3-benzothiazole

Guidance literature:: Multi-step reaction with 6 steps

1: N-iodo-succinimide; trifluoroacetic acid / dichloromethane / 1 h / 20 °C

2: zinc / [2,2]bipyridinyl; nickel dibromide / N,N-dimethyl-formamide / 1 h / 130 °C

3: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

4: lithium hydroxide monohydrate; water / tetrahydrofuran / 1 h / 20 °C

5: thionyl chloride / N,N-dimethyl-formamide / toluene / 16 h / 60 °C

6: triethylamine / chloroform / 1 h / 20 °C

With N-iodo-succinimide; thionyl chloride; lithium hydroxide monohydrate; water; potassium carbonate; triethylamine; trifluoroacetic acid; zinc; [2,2]bipyridinyl; N,N-dimethyl-formamide; nickel dibromide; In tetrahydrofuran; dichloromethane; chloroform; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1285575-21-4
methyl 4-methoxy-3-methylsulfanyl-5-trifluoromethyl benzoate

: 1285575-26-9
3-(4-methoxy-3-methylsulfanyl-5-trifluoromethylbenzoyl)-2,3-dihydro-1,3-benzothiazole

Guidance literature:: Multi-step reaction with 3 steps

1: lithium hydroxide monohydrate; water / tetrahydrofuran / 1 h / 20 °C

2: thionyl chloride / N,N-dimethyl-formamide / toluene / 16 h / 60 °C

3: triethylamine / chloroform / 1 h / 20 °C

With thionyl chloride; lithium hydroxide monohydrate; water; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; chloroform; toluene;