4-(4-Methoxy-phenyl)-1-{2-[2-(4-methoxy-phenyl)-ethyl]-[1,3]dithian-2-yl}-butan-2-ol

Base Information

Chemical Name:4-(4-Methoxy-phenyl)-1-{2-[2-(4-methoxy-phenyl)-ethyl]-[1,3]dithian-2-yl}-butan-2-ol
CAS No.:344249-67-8
Molecular Formula:C₂₄H₃₂O₃S₂
Molecular Weight:432.648
Hs Code.:

Synonyms:4-(4-Methoxy-phenyl)-1-{2-[2-(4-methoxy-phenyl)-ethyl]-[1,3]dithian-2-yl}-butan-2-ol

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Chemical Property of 4-(4-Methoxy-phenyl)-1-{2-[2-(4-methoxy-phenyl)-ethyl]-[1,3]dithian-2-yl}-butan-2-ol

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Technology Process of 4-(4-Methoxy-phenyl)-1-{2-[2-(4-methoxy-phenyl)-ethyl]-[1,3]dithian-2-yl}-butan-2-ol

There total 4 articles about 4-(4-Methoxy-phenyl)-1-{2-[2-(4-methoxy-phenyl)-ethyl]-[1,3]dithian-2-yl}-butan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1929-29-9
3-(4-methoxyphenyl)propanoic acid

: 344249-67-8
4-(4-Methoxy-phenyl)-1-{2-[2-(4-methoxy-phenyl)-ethyl]-[1,3]dithian-2-yl}-butan-2-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 97.5 percent / lithium aluminum hydride / diethyl ether / 1.) 0 deg C, 0.5 h, 2.) 25 deg C, 5 h

2: 83 percent / chromium trioxide, pyridine / CH₂Cl₂ / 0.17 h / 25 °C

3: 94 percent / 1.) boron trifluoride etherate / CH₂Cl₂ / 1.) 0 deg C, 0.5 h, 2.) 25 deg C, 1.5 h

4: 7.6 g / 1.) n-butyllithium / tetrahydrofuran; diethyl ether / 1.) -30 deg C, 1.5 h, 2.) 0 deg C, 12 h

With pyridine; chromium(VI) oxide; lithium aluminium tetrahydride; n-butyllithium; boron trifluoride diethyl etherate; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/ja00411a034

Reference yield:

: 20401-88-1
3-(4-methoxyphenyl)propional

: 344249-67-8
4-(4-Methoxy-phenyl)-1-{2-[2-(4-methoxy-phenyl)-ethyl]-[1,3]dithian-2-yl}-butan-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / 1.) boron trifluoride etherate / CH₂Cl₂ / 1.) 0 deg C, 0.5 h, 2.) 25 deg C, 1.5 h

2: 7.6 g / 1.) n-butyllithium / tetrahydrofuran; diethyl ether / 1.) -30 deg C, 1.5 h, 2.) 0 deg C, 12 h

With n-butyllithium; boron trifluoride diethyl etherate; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/ja00411a034

Reference yield:

: 5406-18-8
3-(p-methoxyphenyl)-1-propanol

: 344249-67-8
4-(4-Methoxy-phenyl)-1-{2-[2-(4-methoxy-phenyl)-ethyl]-[1,3]dithian-2-yl}-butan-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / chromium trioxide, pyridine / CH₂Cl₂ / 0.17 h / 25 °C

2: 94 percent / 1.) boron trifluoride etherate / CH₂Cl₂ / 1.) 0 deg C, 0.5 h, 2.) 25 deg C, 1.5 h

3: 7.6 g / 1.) n-butyllithium / tetrahydrofuran; diethyl ether / 1.) -30 deg C, 1.5 h, 2.) 0 deg C, 12 h

With pyridine; chromium(VI) oxide; n-butyllithium; boron trifluoride diethyl etherate; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/ja00411a034