1,3-Dithiane, 2-[2-(4-methoxyphenyl)ethyl]-

Base Information

Chemical Name:1,3-Dithiane, 2-[2-(4-methoxyphenyl)ethyl]-
CAS No.:56438-60-9
Molecular Formula:C13H18OS2
Molecular Weight:254.417
Hs Code.:
DSSTox Substance ID:DTXSID90481046
Nikkaji Number:J1.930.941J
Wikidata:Q82316248

Synonyms:1,3-Dithiane, 2-[2-(4-methoxyphenyl)ethyl]-;56438-60-9;DTXSID90481046

Suppliers and Price of 1,3-Dithiane, 2-[2-(4-methoxyphenyl)ethyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,3-Dithiane, 2-[2-(4-methoxyphenyl)ethyl]-

Chemical Property:

XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:254.07990754
Heavy Atom Count:16
Complexity:184

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)CCC2SCCCS2

Technology Process of 1,3-Dithiane, 2-[2-(4-methoxyphenyl)ethyl]-

There total 8 articles about 1,3-Dithiane, 2-[2-(4-methoxyphenyl)ethyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5406-18-8
3-(p-methoxyphenyl)-1-propanol

: 56438-60-9
2-[2-(4-methoxyphenyl)ethyl]-1,3-dithiane

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / chromium trioxide, pyridine / CH₂Cl₂ / 0.17 h / 25 °C

2: 94 percent / 1.) boron trifluoride etherate / CH₂Cl₂ / 1.) 0 deg C, 0.5 h, 2.) 25 deg C, 1.5 h

With pyridine; chromium(VI) oxide; boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1021/ja00411a034

Reference yield:

: 1929-29-9
3-(4-methoxyphenyl)propanoic acid

: 56438-60-9
2-[2-(4-methoxyphenyl)ethyl]-1,3-dithiane

Guidance literature:: Multi-step reaction with 3 steps

1: 97.5 percent / lithium aluminum hydride / diethyl ether / 1.) 0 deg C, 0.5 h, 2.) 25 deg C, 5 h

2: 83 percent / chromium trioxide, pyridine / CH₂Cl₂ / 0.17 h / 25 °C

3: 94 percent / 1.) boron trifluoride etherate / CH₂Cl₂ / 1.) 0 deg C, 0.5 h, 2.) 25 deg C, 1.5 h

With pyridine; chromium(VI) oxide; lithium aluminium tetrahydride; boron trifluoride diethyl etherate; In diethyl ether; dichloromethane;
DOI:10.1021/ja00411a034

Reference yield:

: 634-36-6
1,2,3-trimethoxybenzene

: 56438-60-9
2-[2-(4-methoxyphenyl)ethyl]-1,3-dithiane

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) aluminium chloride, 2.) sodium dithionite, sodium hydroxide / 1.) 1,1,2,2-tetrachloroethane, room temperature, 16 h; steam-bath, 2 h, 2.) methanol, room temperature, 21 h, reflux, 24 h

2: 88 percent / hydrogen / palladium-carbon / acetic acid / 1.5 h / Ambient temperature

3: 59 percent / lithium aluminium hydride / diethyl ether

4: 62 percent / pyridine

5: 80 percent / lithium bromide / acetone / 24 h / Ambient temperature

6: magnesium (from magnesium chloride and potassium metal, 3-(4-methoxyphenyl)propanal / tetrahydrofuran

7: 74 percent / pyridinium chlorochromate / CH₂Cl₂ / 4.5 h

8: 54 percent / hydrogen chloride / CH₂Cl₂ / 0.5 h / -25 °C

With pyridine; hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; aluminium trichloride; sodium dithionite; 3-(4-methoxyphenyl)propional; hydrogen; magnesium; pyridinium chlorochromate; lithium bromide; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; dichloromethane; acetic acid; acetone;