Technology Process of C24H25ClO6S
There total 10 articles about C24H25ClO6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Dess-Martin periodane;
In
dichloromethane;
at 0 - 20 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrabutyl-ammonium chloride / toluene / 18 h / 40 °C
2: di-isopropyl azodicarboxylate; triphenylphosphine / dichloromethane / 18 h / 20 °C
3: methanol / pyridinium p-toluenesulfonate / 20 - 40 °C
4: Dess-Martin periodane / dichloromethane / 0 - 20 °C
With
methanol; di-isopropyl azodicarboxylate; tetrabutyl-ammonium chloride; Dess-Martin periodane; triphenylphosphine;
pyridinium p-toluenesulfonate;
In
dichloromethane; toluene;
2: Mitsunobu reaction;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 6 h
2: triethylamine / dichloromethane / 0 - 20 °C
3: tetrabutyl-ammonium chloride / toluene / 18 h / 40 °C
4: di-isopropyl azodicarboxylate; triphenylphosphine / dichloromethane / 18 h / 20 °C
5: methanol / pyridinium p-toluenesulfonate / 20 - 40 °C
6: Dess-Martin periodane / dichloromethane / 0 - 20 °C
With
methanol; di-isopropyl azodicarboxylate; tetrabutyl-ammonium chloride; hydrogen; Dess-Martin periodane; triethylamine; triphenylphosphine;
palladium 10% on activated carbon; pyridinium p-toluenesulfonate;
In
dichloromethane; ethyl acetate; toluene;
4: Mitsunobu reaction;
