benzoxazolyl 3,4-di-O-acetyl-2-O-benzyl-6-O-(3-hydroxycarbonylpropanoyl)-β-D-glucopyranoside

Base Information

Chemical Name:benzoxazolyl 3,4-di-O-acetyl-2-O-benzyl-6-O-(3-hydroxycarbonylpropanoyl)-β-D-glucopyranoside
CAS No.:1012046-48-8
Molecular Formula:C₂₈H₂₉NO₁₁S
Molecular Weight:587.604
Hs Code.:

Synonyms:benzoxazolyl 3,4-di-O-acetyl-2-O-benzyl-6-O-(3-hydroxycarbonylpropanoyl)-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzoxazolyl 3,4-di-O-acetyl-2-O-benzyl-6-O-(3-hydroxycarbonylpropanoyl)-β-D-glucopyranoside

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Technology Process of benzoxazolyl 3,4-di-O-acetyl-2-O-benzyl-6-O-(3-hydroxycarbonylpropanoyl)-β-D-glucopyranoside

There total 1 articles about benzoxazolyl 3,4-di-O-acetyl-2-O-benzyl-6-O-(3-hydroxycarbonylpropanoyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 862537-78-8
benzoxazol-2-yl 3,4-di-O-acetyl-2-O-benzyl-1-thio-β-D-glucopyranoside

: 108-30-5
succinic acid anhydride

: 1012046-48-8
benzoxazolyl 3,4-di-O-acetyl-2-O-benzyl-6-O-(3-hydroxycarbonylpropanoyl)-β-D-glucopyranoside

Guidance literature:: With pyridine; dmap; at 20 ℃; for 16h;
DOI:10.1021/jo701902f

Reference yield: 54.0%

: 53008-65-4,641635-63-4
methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

: 1012046-48-8
benzoxazolyl 3,4-di-O-acetyl-2-O-benzyl-6-O-(3-hydroxycarbonylpropanoyl)-β-D-glucopyranoside

: 1012046-26-2
C₄₁H₄₈O₁₁

Guidance literature:: benzoxazolyl 3,4-di-O-acetyl-2-O-benzyl-6-O-(3-hydroxycarbonylpropanoyl)-β-D-glucopyranoside; With dicyclohexyl-carbodiimide; In dichloromethane; for 72h;

methyl 2,3,4-tri-O-benzyl-D-glucopyranoside; With 3 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 96h;

With methanol; sodium methylate; In dichloromethane; at 20 ℃; for 48h; pH=8 - 9; Further stages.;
DOI:10.1021/jo701902f

Reference yield:

: 1012046-48-8
benzoxazolyl 3,4-di-O-acetyl-2-O-benzyl-6-O-(3-hydroxycarbonylpropanoyl)-β-D-glucopyranoside

: 35784-51-1
ethyl 2,3,4-tri-O-benzoyl-1-thio-β-D-glucopyranoside

: C₂₁H₃₂O₁₀S

Guidance literature:: benzoxazolyl 3,4-di-O-acetyl-2-O-benzyl-6-O-(3-hydroxycarbonylpropanoyl)-β-D-glucopyranoside; With dicyclohexyl-carbodiimide; In dichloromethane; for 72h;

ethyl 2,3,4-tri-O-benzoyl-1-thio-β-D-glucopyranoside; With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; at 20 ℃; for 96h;

With methanol; sodium methylate; In dichloromethane; at 20 ℃; for 48h; pH=8 - 9; Further stages.;
DOI:10.1021/jo701902f