3,4,6-tri-O-acetyl-2-deoxy-2-otrifluoromethylbenzylideneamino-D-glucopyranosyl N-phenyl trifluoroacetimidate

Base Information

Chemical Name:3,4,6-tri-O-acetyl-2-deoxy-2-otrifluoromethylbenzylideneamino-D-glucopyranosyl N-phenyl trifluoroacetimidate
CAS No.:1391597-82-2
Molecular Formula:C₂₈H₂₆F₆N₂O₈
Molecular Weight:632.513
Hs Code.:

Synonyms:3,4,6-tri-O-acetyl-2-deoxy-2-otrifluoromethylbenzylideneamino-D-glucopyranosyl N-phenyl trifluoroacetimidate

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Chemical Property of 3,4,6-tri-O-acetyl-2-deoxy-2-otrifluoromethylbenzylideneamino-D-glucopyranosyl N-phenyl trifluoroacetimidate

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Technology Process of 3,4,6-tri-O-acetyl-2-deoxy-2-otrifluoromethylbenzylideneamino-D-glucopyranosyl N-phenyl trifluoroacetimidate

There total 1 articles about 3,4,6-tri-O-acetyl-2-deoxy-2-otrifluoromethylbenzylideneamino-D-glucopyranosyl N-phenyl trifluoroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: triacetyl D-glucosamine hemiacetal

: 61881-19-4
2,2,2-trifluoro-N-phenyl-acetimidoyl chloride

: 1391597-82-2
3,4,6-tri-O-acetyl-2-deoxy-2-otrifluoromethylbenzylideneamino-D-glucopyranosyl N-phenyl trifluoroacetimidate

: 1391597-83-3
3,4,6-tri-O-acetyl-2-deoxy-2-otrifluoromethylbenzylideneamino-D-glucopyranosyl N-phenyl trifluoroacetimidate

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃; Overall yield = 80 %; Overall yield = 5.26 g;
DOI:10.1021/jo301050q

Reference yield: 93.0%

: 1391597-81-1
C₁₆H₁₉F₃O₄S

: 1391597-82-2
3,4,6-tri-O-acetyl-2-deoxy-2-otrifluoromethylbenzylideneamino-D-glucopyranosyl N-phenyl trifluoroacetimidate

: 1391598-29-0
2-trifluorophenyl 3,4,6-tri-O-acetyl-2-deoxy-2-o-trifluoromethylbenzylideneamino-α-D-glucopyranosyl-(1→4)-2,3-di-O-isopropylidene-1-thiol-α-L-rhamnopyranoside

Guidance literature:: With nickel(II) triflate; In dichloromethane; at 35 ℃; for 16h; Inert atmosphere;
DOI:10.1016/j.carres.2016.10.008

Reference yield: 77.0%

: 1391597-82-2
3,4,6-tri-O-acetyl-2-deoxy-2-otrifluoromethylbenzylideneamino-D-glucopyranosyl N-phenyl trifluoroacetimidate

: 1432469-19-6
C₃₁H₃₄O₈

: 1432469-23-2
C₅₁H₅₄F₃NO₁₅

Guidance literature:: With Ni(4-F-PhCN)₄Cl₂; silver trifluoromethanesulfonate; In dichloromethane; at 35 ℃; for 4h; diastereoselective reaction; Inert atmosphere;
DOI:10.1039/c2cc35823a