Technology Process of 6-methyl-8t-(2,6,6-trimethyl-cyclohex-1-enyl)-octa-3t,5c,7-trien-2-one semicarbazone
There total 6 articles about 6-methyl-8t-(2,6,6-trimethyl-cyclohex-1-enyl)-octa-3t,5c,7-trien-2-one semicarbazone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: zinc; benzene / nach Behandeln mit wss. Essigsaeure Erwaermen mit Oxalsaeure unter vermind. Druck und Behandeln des nach der Destillation bei 120-160grad/0.001 Torr erhaltenen Ester-Gemisches mit wss.-aethanol. Kalilauge bzw. aethanol. Kalilauge
2: diethyl ether
With
diethyl ether; zinc; benzene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: zinc; diethyl ether; tetrahydrofuran / Hydrolyse und Dehydratisierung mit Hilfe von N-Jod-succinimid
2: diethyl ether
With
tetrahydrofuran; diethyl ether; zinc;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: diethyl ether
With
diethyl ether;