2-cyanobenzo[d]thiazol-6-yl (3-(N,3-dimethyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamido)propyl)carbonate

Base Information

Chemical Name:2-cyanobenzo[d]thiazol-6-yl (3-(N,3-dimethyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamido)propyl)carbonate
CAS No.:1426551-50-9
Molecular Formula:C₂₇H₂₉N₃O₆S
Molecular Weight:523.61
Hs Code.:

Synonyms:2-cyanobenzo[d]thiazol-6-yl (3-(N,3-dimethyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamido)propyl)carbonate

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Chemical Property of 2-cyanobenzo[d]thiazol-6-yl (3-(N,3-dimethyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamido)propyl)carbonate

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Technology Process of 2-cyanobenzo[d]thiazol-6-yl (3-(N,3-dimethyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamido)propyl)carbonate

There total 6 articles about 2-cyanobenzo[d]thiazol-6-yl (3-(N,3-dimethyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamido)propyl)carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1426551-49-6
C₁₉H₂₆ClNO₅

: 939-69-5
2-cyano-6-hydroxybenzothiazole

: 1426551-50-9
2-cyanobenzo[d]thiazol-6-yl (3-(N,3-dimethyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamido)propyl)carbonate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 2h;

Reference yield:

: 1426551-48-5
N-(3-hydroxypropyl)-N,3-dimethyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamide

: 1426551-50-9
2-cyanobenzo[d]thiazol-6-yl (3-(N,3-dimethyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamido)propyl)carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 0.5 h / 0 - 20 °C

2: triethylamine / tetrahydrofuran / 2 h / 0 - 20 °C

With pyridine; triethylamine; In tetrahydrofuran; dichloromethane;

Reference yield:

: 924-50-5
Methyl 3,3-dimethylacrylate

: 1426551-50-9
2-cyanobenzo[d]thiazol-6-yl (3-(N,3-dimethyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamido)propyl)carbonate

Guidance literature:: Multi-step reaction with 5 steps

1.1: methanesulfonic acid / 2 h / 70 °C

2.1: N-Bromosuccinimide; water / acetonitrile; acetone / 0.5 h / 20 °C

3.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 0.5 h / 0 °C

3.2: 20 °C

4.1: pyridine / dichloromethane / 0.5 h / 0 - 20 °C

5.1: triethylamine / tetrahydrofuran / 2 h / 0 - 20 °C

With 4-methyl-morpholine; pyridine; N-Bromosuccinimide; methanesulfonic acid; water; triethylamine; isobutyl chloroformate; In tetrahydrofuran; dichloromethane; acetone; acetonitrile;