((S,Z)-(+)-3-(butyltellanyl)-1-phenylallyloxy)(tert-butyl)dimethylsilane

Base Information

• Chemical Name: ((S,Z)-(+)-3-(butyltellanyl)-1-phenylallyloxy)(tert-butyl)dimethylsilane
• CAS No.: 835594-86-0
• Molecular Formula: C₁₉H₃₂OSiTe
• Molecular Weight: 432.148

Synonyms:((S,Z)-(+)-3-(butyltellanyl)-1-phenylallyloxy)(tert-butyl)dimethylsilane

Chemical Property of ((S,Z)-(+)-3-(butyltellanyl)-1-phenylallyloxy)(tert-butyl)dimethylsilane

Chemical Property:

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Technology Process of ((S,Z)-(+)-3-(butyltellanyl)-1-phenylallyloxy)(tert-butyl)dimethylsilane

There total 3 articles about ((S,Z)-(+)-3-(butyltellanyl)-1-phenylallyloxy)(tert-butyl)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

n-butyllithium (109-72-8,29786-93-4) + (S)-(+)-(1-phenyl-prop-2-ynyloxy)(tert-butyl)dimethylsilane (835594-85-9) → ((S,Z)-(+)-3-(butyltellanyl)-1-phenylallyloxy)(tert-butyl)dimethylsilane (835594-86-0)

Guidance literature:

n-butyllithium; With tellurium; In tetrahydrofuran; hexane; at 20 ℃; for 0.0833333h;

(S)-(+)-(1-phenyl-prop-2-ynyloxy)(tert-butyl)dimethylsilane; In tetrahydrofuran; ethanol; hexane; Heating;

DOI:10.1016/j.tet.2004.10.087

Reference yield:

1-phenylprop-2-yn-1-ol (4187-87-5,61317-73-5,64937-86-6,64599-56-0) → ((S,Z)-(+)-3-(butyltellanyl)-1-phenylallyloxy)(tert-butyl)dimethylsilane (835594-86-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 80 percent / imidazole / CHCl₃ / 12 h / 20 °C

2.1: tellurium / tetrahydrofuran; hexane / 0.08 h / 20 °C

2.2: 72 percent / tetrahydrofuran; hexane; ethanol / Heating

With 1H-imidazole; tellurium; In tetrahydrofuran; hexane; chloroform;

DOI:10.1016/j.tet.2004.10.087

Reference yield:

tert-butyldimethylsilyl chloride (18162-48-6) → ((S,Z)-(+)-3-(butyltellanyl)-1-phenylallyloxy)(tert-butyl)dimethylsilane (835594-86-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 80 percent / imidazole / CHCl₃ / 12 h / 20 °C

2.1: tellurium / tetrahydrofuran; hexane / 0.08 h / 20 °C

2.2: 72 percent / tetrahydrofuran; hexane; ethanol / Heating

With 1H-imidazole; tellurium; In tetrahydrofuran; hexane; chloroform;

DOI:10.1016/j.tet.2004.10.087

upstream raw materials:

n-butyllithium

(S)-(+)-(1-phenyl-prop-2-ynyloxy)(tert-butyl)dimethylsilane

1-phenylprop-2-yn-1-ol

tert-butyldimethylsilyl chloride

Downstream raw materials:

((S,Z)-(+)-1-phenyl-dec-2-en-4-ynyloxy)(tert-butyl)dimethylsilane

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