(4S)-1-[(2S,3S)-3-(N₂-t-butoxycarbonyl-L-asparaginyl)amino-2-hydroxy-4-phenylbutyryl]-4-chloro-N-t-butyl-L-prolinamide

Base Information

• Chemical Name: (4S)-1-[(2S,3S)-3-(N₂-t-butoxycarbonyl-L-asparaginyl)amino-2-hydroxy-4-phenylbutyryl]-4-chloro-N-t-butyl-L-prolinamide
• CAS No.: 166383-31-9
• Molecular Formula: C₂₈H₄₂ClN₅O₇
• Molecular Weight: 596.124

Synonyms:(4S)-1-[(2S,3S)-3-(N₂-t-butoxycarbonyl-L-asparaginyl)amino-2-hydroxy-4-phenylbutyryl]-4-chloro-N-t-butyl-L-prolinamide

Chemical Property of (4S)-1-[(2S,3S)-3-(N₂-t-butoxycarbonyl-L-asparaginyl)amino-2-hydroxy-4-phenylbutyryl]-4-chloro-N-t-butyl-L-prolinamide

Chemical Property:

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Technology Process of (4S)-1-[(2S,3S)-3-(N₂-t-butoxycarbonyl-L-asparaginyl)amino-2-hydroxy-4-phenylbutyryl]-4-chloro-N-t-butyl-L-prolinamide

There total 1 articles about (4S)-1-[(2S,3S)-3-(N₂-t-butoxycarbonyl-L-asparaginyl)amino-2-hydroxy-4-phenylbutyryl]-4-chloro-N-t-butyl-L-prolinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4S)-1-[(2S,3S)-3-amino-2-hydroxy-4-phenylbutyryl]-4-chloro-N-t-butyl-L-prolinamide (166383-81-9) → (4S)-1-[(2S,3S)-3-(N2-t-butoxycarbonyl-L-asparaginyl)amino-2-hydroxy-4-phenylbutyryl]-4-chloro-N-t-butyl-L-prolinamide (166383-31-9)

Guidance literature:

With sodium hydroxide; sodium chloride; triethylamine; citric acid; In N-methyl-acetamide;

Reference yield:

(4S)-1-[(2S,3S)-3-(N2-t-butoxycarbonyl-L-asparaginyl)amino-2-hydroxy-4-phenylbutyryl]-4-chloro-N-t-butyl-L-prolinamide (166383-31-9) + 7-methoxybenzofuran-2-carboxylic acid (4790-79-8) → (4S)-1-{(2S,3S)-3-(N2-(7-Methoxy-2-benzofurancarbonyl)-L-asparaginyl]amino-2-hydroxy-4-phenylbutyryl}-4-chloro-N-t-butyl-L-prolinamide

Guidance literature:

upstream raw materials:

(4S)-1-[(2S,3S)-3-amino-2-hydroxy-4-phenylbutyryl]-4-chloro-N-t-butyl-L-prolinamide

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